Porous light honeycomb zeolite and preparation method thereof
A lightweight, honeycomb technology, applied in the field of honeycomb zeolite, can solve the problems of low bulk density, poor molding and shaping effect, increase of honeycomb zeolite bulk density, etc., and achieve the effects of reducing bulk density, increasing the number of pores, and increasing the contact area.
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Embodiment 1
[0024] A method for preparing a porous lightweight honeycomb zeolite provided in an embodiment of the present invention may include the following steps:
[0025] Quantitative weighing: Weigh all the raw materials according to the designed ratio.
[0026] Mixing of main ingredients: add the weighed main ingredients into a twin-screw mixer and mix for 2-3 hours.
[0027] Mud mixing: Mix the mixed mud evenly with a mud mixer.
[0028] Stale mud: Seal and stale the kneaded mud, and spread the water evenly to eliminate the internal stress of the mud.
[0029] Extrusion molding: Extrude molding with a honeycomb extruder, and cut samples according to the pre-designed size.
[0030] Drying and sintering: After 4-5 days in a closed and windless condition, put the sample into a microwave oven for drying, control the moisture content below 3% and put it into the furnace for sintering.
[0031] In this embodiment, the porous lightweight honeycomb zeolite may include: 40% diatomite, 20%...
Embodiment 2
[0033] A method for preparing a porous lightweight honeycomb zeolite provided in an embodiment of the present invention may include the following steps:
[0034] Quantitative weighing: Weigh all the raw materials according to the designed ratio.
[0035] Mixing of main ingredients: add the weighed main ingredients into a twin-screw mixer and mix for 2-3 hours.
[0036] Mud mixing: Mix the mixed mud evenly with a mud mixer.
[0037] Stale mud: Seal and stale the kneaded mud, and spread the water evenly to eliminate the internal stress of the mud.
[0038] Extrusion molding: Extrude molding with a honeycomb extruder, and cut samples according to the pre-designed size.
[0039] Drying and sintering: After 4-5 days in a closed and windless condition, put the sample into a microwave oven for drying, control the moisture content below 3% and put it into the furnace for sintering.
[0040] In this embodiment, the porous lightweight honeycomb zeolite includes: 45% diatomite, 15% li...
Embodiment 3
[0042] A method for preparing a porous lightweight honeycomb zeolite provided in an embodiment of the present invention may include the following steps:
[0043] Quantitative weighing: Weigh all the raw materials according to the designed ratio.
[0044] Mixing of main ingredients: add the weighed main ingredients into a twin-screw mixer and mix for 2-3 hours.
[0045] Mud mixing: Mix the mixed mud evenly with a mud mixer.
[0046] Stale mud: Seal and stale the kneaded mud, and spread the water evenly to eliminate the internal stress of the mud.
[0047] Extrusion molding: Extrude molding with a honeycomb extruder, and cut samples according to the pre-designed size.
[0048] Drying and sintering: After 4-5 days in a closed and windless condition, put the sample into a microwave oven for drying, control the moisture content below 3% and put it into the furnace for sintering.
[0049] In this embodiment, the porous lightweight honeycomb zeolite includes: 47% of diatomite, 13%...
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