Poly (alkylene carbonate)-based resin and molded article manufactured therefrom
A technology of polyalkylene carbonate and molded products, applied in the field of molded products, can solve problems such as reducing transparency, achieve excellent gas barrier properties, excellent thermal stability, and improve the effect of heat shrinkage
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preparation example 1
[0080] In a glove box, the organozinc catalyst and methylene chloride were added to the high pressure reactor, followed by ethylene oxide. Subsequently, carbon dioxide was added thereto, and then a polymerization reaction was performed at 70° C. for 3 hours to prepare polyethylene carbonate having a weight average molecular weight of 140,000 g / mol. After the reaction, unreacted carbon dioxide, unreacted ethylene oxide and dichloromethane solvent were removed together, and pellets (diameter: 3 mm, thickness: 3 mm) were prepared using the prepared polyethylene carbonate with an extruder. ). The prepared polyethylene carbonate (Mw 140,000g / mol) pellets and polylactide resin (PLA2003D, NatureWorks Co., Ltd) were shaken at room temperature (23±5°C) at a weight ratio of 5:5 to Mix well, then place the mixture in a vacuum oven at 40°C overnight. Then, a pellet-shaped base resin was prepared using an extruder.
reference example 1
[0082] Except in Preparation Example 1, polyethylene carbonate (Mw 140,000 g / mol) pellets and polylactide resin (PLA 2003D, NatureWorks Co., Ltd) were mixed in a weight ratio of 7:3 instead of a weight ratio of 5 :5 mixed to prepare the base resin, in the same manner as in Preparation Example 1, Reference Example 1 was carried out.
reference example 2
[0084] Except in Preparation Example 1, polyethylene carbonate (Mw 140,000 g / mol) pellets and polylactide resin (PLA 2003D, NatureWorks Co., Ltd) were mixed in a weight ratio of 3:7 instead of a weight ratio of 5 :5 mixed to prepare the base resin, in the same manner as in Preparation Example 1, Reference Example 1 was carried out.
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