Releasing agent for plastics
A release agent and plastic technology, applied in the field of organopolysiloxane emulsion composition, can solve the problems of molded body cracks, uneven coating, cracks, etc., and achieve the effect of good storage stability and excellent wettability
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[0131] [Preparation of composition]
[0132]An example of a specific production method of the release agent for plastics of the present invention is mainly shown below.
[0133] (A) organopolysiloxane, (B) anionic surfactant, (C) polyoxyethylene alkyl ether, (D) polyoxyethylene sorbitan fatty acid ester, (F) sorbose After a part of alcohol anhydride fatty acid ester and (E) water was stirred and emulsified, it diluted with the remaining (E) water. When the (A) component is not easily emulsified, it can be easily emulsified by adding a part of each of (A) to (D) components, (F) component and a part of (E) component and stirring, adding The remaining (A) - (D) components and (F) components are further stirred. Especially when the viscosity of component (A) is less than 1,000mm 2 / s, (A) component may be difficult to emulsify. In such a case, emulsification can be easily performed by adding (A)-(D) component and (F) component in portions. A specific example of an emulsified ...
Embodiment 1
[0146] [chemical formula 9]
[0147]
[0148] 30 parts by mass (90 g) of (A) component [1] organopolysiloxane (1a) represented by the above formula was stirred with HOMO DISPER MODEL 2.5 (manufactured by PRIMIX Corporation) at 500 rpm (L1 is about 550, viscosity is 10,000 mm 2 / s), 0.2 parts by mass (0.6g) of (B) component [1] EMAL 270J (manufactured by Kao Corporation, 70% aqueous solution of polyoxyethylene alkyl ether sodium sulfate), 6.0 parts by mass (18g) of (C) Component [1] LEOCOL TDN90-80 (2a) (manufactured by Lion Specialty Chemicals Co., Ltd., 80% aqueous solution of polyoxyethylene alkyl ether), 1.6 parts by mass (4.8 g) of (D) component [1] NONION LT -221 (manufactured by NOF CORPORATION, polyoxyethylene sorbitan monolaurate), 0.4 parts by mass (1.2 g) of (F) component NONION LP-20R (manufactured by NOF CORPORATION, sorbitan monolaurate) And 1.5 mass parts (4.5g) of water as (E)-1 component, after emulsifying the whole, stir with 1,500rpm for 20 minutes, then...
Embodiment 2
[0150] 30 parts by mass (90 g) of (A) component [1] organopolysiloxane (1a) (L1 is about 550, viscosity is 10,000 mm 2 / s), 1.3 parts by mass (3.9g) of (B) component [1] EMAL 270J (manufactured by Kao Corporation, 70% aqueous solution of polyoxyethylene alkyl ether sodium sulfate), 6.0 parts by mass (18g) of (C) Component [1] LEOCOL TDN90-80 (2a) (manufactured by Lion Specialty Chemicals Co., Ltd., 80% aqueous solution of polyoxyethylene alkyl ether), 1.6 parts by mass (4.8 g) of (D) component [1] NONIONLT- 221 (manufactured by NOF CORPORATION, polyoxyethylene sorbitan monolaurate), 0.4 parts by mass (1.2 g) of (F) component NONION LP-20R (manufactured by NOF CORPORATION, sorbitan monolaurate) and 1.0 parts by mass (3.0g) of water as component (E)-1 was emulsified as a whole, stirred at 1,500rpm for 20 minutes, then 59.55 parts by mass (178.65g) of water as component (E)-2 was added, and used HOMO MIXER MARKII MODEL 2.5 (manufactured by PRIMIX Corporation) was stirred at 1,50...
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