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A composite thermal insulation pad and its manufacturing process

A manufacturing process and a technology for thermal insulation pads, applied in the field of heat-resistant materials, can solve the problems of limiting the application of pure silica aerogel, serious aerogel cracking, poor integrity, etc., achieving low environmental damage, high insulation performance, Long service life effect

Active Publication Date: 2022-08-05
重庆智笃新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to SiO 2 The characteristics of airgel, such as low density, irregular pore structure, disordered three-dimensional network morphology and dense agglomeration to form a density gradient, lead to SiO 2 Airgel cracking is relatively serious and its integrity is poor, which limits the application of pure silica aerogels
In SiO 2 In the field of airgel and fiber composites, fibers such as glass fibers, mullite fibers and quartz fibers are commonly used in the form of chopped fibers or fiber mats with SiO 2 Airgel is composited, and it is difficult to use it in a higher temperature (above 300°C) environment due to the defects of the fiber itself

Method used

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  • A composite thermal insulation pad and its manufacturing process

Examples

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Effect test

Embodiment 1

[0041] A manufacturing process of a composite thermal insulation pad, the manufacturing process of the thermal insulation pad comprises the following steps: figure 1 shown,

[0042] S1. Prepare aerogel precursor hydrolyzate: select 50 grams of orthosilicate and a hydrolyzing agent (100 grams of deionized water and 300 grams of anhydrous ethanol) according to the proportion and mix, first add hydrochloric acid solution to adjust the pH value to 3-5 , carry out the first stirring for 15 minutes, then add ammonia water to adjust the pH value to 7-8, and carry out the second stirring for 15 minutes to obtain aerogel precursor hydrolyzate;

[0043] S2. Impregnation substrate: The basalt fiber needle-punched felt substrate with a thickness of 1 mm is placed in the aerogel precursor hydrolyzate for 30 seconds through the unwinder, and then the aerogel precursor is squeezed and wound through the winder. The basalt fiber needle-punched felt base material after the hydrolyzate is obtai...

Embodiment 2

[0046] A manufacturing process of a composite thermal insulation pad, the manufacturing process of the thermal insulation pad comprises the following steps: figure 1 shown,

[0047] S1. Prepare aerogel precursor hydrolyzate: select 200 grams of orthosilicate and a hydrolyzing agent (500 grams of deionized water and 850 grams of anhydrous ethanol) according to the corresponding proportions and mix, first add hydrochloric acid solution to adjust the pH to 3- 5. Carry out the first stirring for 60 minutes, then add ammonia water to adjust the pH to 7-8, and carry out the second stirring for 60 minutes to obtain aerogel precursor hydrolyzate;

[0048] S2. Impregnation substrate: The basalt fiber needle-punched felt substrate with a thickness of 20 mm is placed in the hydrolyzed solution of the aerogel precursor for 120 seconds through the unwinder, and then the aerogel precursor is squeezed and wound through the winder. The basalt fiber needle-punched felt base material after the...

Embodiment 3

[0051] A manufacturing process of a composite thermal insulation pad, the manufacturing process of the thermal insulation pad comprises the following steps: figure 1 shown,

[0052] S1, prepare aerogel precursor hydrolyzate: select 50 grams of orthosilicate and hydrolyzing agent (100 grams of deionized water and 300 grams of absolute ethanol) according to the corresponding proportion, mix well, first add hydrochloric acid solution to adjust the pH value to 3- 5. Carry out the first stirring for 15 minutes, then add ammonia water to adjust the pH to 7-8, and carry out the second stirring for 60 minutes to obtain aerogel precursor hydrolyzate;

[0053] S2. Impregnation substrate: The basalt fiber needle-punched felt substrate with a thickness of 1 mm is placed in the aerogel precursor hydrolyzate for 30 seconds through the unwinder, and then the aerogel precursor is squeezed and wound through the winder. The basalt fiber needle-punched felt base material after the hydrolyzate i...

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Abstract

The invention belongs to the technical field of heat-resistant materials, and discloses a composite thermal insulation pad and a manufacturing process thereof. Using the ultra-fine basalt fiber needle-punched felt as the raw material, an ultra-thin (1mm thick) ultra-fine basalt fiber aerogel composite thermal insulation pad can be prepared, which can be used in the field of high-temperature thermal insulation materials for power batteries. A product with higher temperature resistance and lower thermal conductivity is prepared and obtained, which not only has better thermal insulation performance, but also has higher insulation performance, longer service life and less environmental hazard. The ultra-fine basalt fiber aerogel composite thermal insulation pad can be used as a thermal insulation material with better performance and can be widely used in metallurgy, machinery, electric power, chemical thermal equipment, aerospace, and military fields. The supercritical method is used to directly dry the aged ultrafine basalt fiber needled felt to obtain a gel-like ultrafine basalt fiber needled felt, which saves the step of replacing the solvent, improves the production efficiency, and shortens the drying time. Reduced production costs.

Description

technical field [0001] The invention belongs to the technical field of heat-resistant materials, and in particular relates to a composite thermal insulation pad and a manufacturing process thereof. Background technique [0002] With the development of inorganic ceramic fiber materials, various SiO 2 , Al 2 O 3 This material does not expand when heated, has good heat insulation, and is resistant to high temperature thermal shock, so it is widely used in industrial installations or high temperature combustion furnaces. hot. In addition, it is also widely used in aerospace thermal protection engineering. However, due to the properties of its material, the theoretical thermal conductivity of the heat resistance coefficient is between 0.045W / (m·K) and 0.210W / (m·K). Due to SiO 2 The low density, irregular pore structure, disordered three-dimensional network morphology, and dense agglomeration of aerogels form density gradients, which lead to SiO 2 The aerogel has serious cr...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B30/02
CPCC04B30/02C04B2201/32C04B14/4643C04B14/064
Inventor 肖尧刘云跃
Owner 重庆智笃新材料科技有限公司
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