Nano-composite carbon nitride catalytic material and preparation method and application thereof
A technology for compounding carbon nitride and catalytic materials, which is applied in the field of preparation and application of catalytic materials, can solve problems such as narrow visible light response range, and achieve the effects of high catalytic activity, simplified production process, and reduced production cost.
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0033] Grind 30g of melamine evenly and put it into a crucible with a cover, and place the crucible in a muffle furnace for roasting. The muffle furnace heats up to 700°C at a rate of 2°C / min, keeps it warm for 4h, and cools naturally to obtain carbon nitride . carbon nitride, C 60 , Deionized water is placed in a ball mill according to the mass ratio of 5:0.1:8, ball milled at a speed of 300 rpm, kept for 8 hours, and the nanocomposite carbon nitride material is obtained after drying, which is recorded as CN-700-C 60 .
[0034] C prepared for testing this example 60 / g -C 3 N 4 For the photocatalytic performance of the material, the material prepared in this example was used in the red photocatalytic degradation of Rhodamine B (RhB) to test its photocatalytic activity. Measure the Rhodamine B aqueous solution of 50mL 10μg / mL and put it into a test tube, add 0.03g of C prepared in this embodiment 60 / g -C 3 N 4, with a wavelength of 660nm, a power of 50W LED lamp as a ...
Embodiment 2
[0036] Grind 30g of melamine evenly and put it into a crucible with a cover, and place the crucible in a muffle furnace for roasting. The muffle furnace heats up to 700°C at a rate of 2°C / min, keeps it warm for 4h, and cools naturally to obtain carbon nitride . carbon nitride, C 60 1. Deionized water was placed in a ball mill at a mass ratio of 5:0.05:8, ball milled at a rate of 300 rpm, kept for 8 hours, and dried to obtain a nanocomposite carbon nitride material.
[0037] The C prepared in this embodiment 60 / g -C 3 N 4 The material is used in the reaction of red light (660nm) to catalyze the degradation of rhodamine B, the reaction conditions are the same as in Example 1, the light is 90min, and the degradation rate is 1.399h -1 .
Embodiment 3
[0039] Grind 30g of melamine evenly and put it into a crucible with a cover, and place the crucible in a muffle furnace for roasting. The muffle furnace heats up to 550°C at a rate of 2°C / min, keeps it warm for 3 hours, and cools naturally to obtain carbon nitride . carbon nitride, C 60 1. Deionized water was placed in a ball mill at a mass ratio of 5:0.15:8, ball milled at a rate of 400 rpm, kept for 7 hours, and dried to obtain a nanocomposite carbon nitride material.
[0040] The C prepared in this embodiment 60 / g -C 3 N 4 The material is used in the reaction of red light (660nm) to catalyze the degradation of rhodamine B, the reaction conditions are the same as in Example 1, the light is 90min, and the degradation rate is 1.097h -1 .
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More