Mask outer packaging bag capable of invalidating regularly and production method thereof
A timing failure and outer packaging bag technology, applied in the field of packaging bags, can solve problems such as environmental pollution, mask packaging bag corrosion, mask pollution, etc.
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Embodiment 1
[0059] This example is a method of preparing an antibacterial hydrophobic resin comprising the steps of:
[0060] Step 1: 0.03 mol of dichlorosulfoxide, 0.01 g of the polymerization agent is added to the three flask mounted to a thermometer, a condensate return tube, a constant voltage drip funnel, and a stirrer, stirring at a temperature of 10 ° C, stirring The rate of 0.1 mol acrylic acid was added dropwise over the conditions of 200R / min, and the drip rate was 1 drop / s, and the reaction was refluxed after the dropping temperature of 40 ° C, and the reaction product was cooled after the reaction was completed. At room temperature, the fraction of 30 ° C was collected under pressure of 18.7 kPa, and an intermediate 1 was collected under conditions of 18.7 kPa.
[0061] Step 2: 0.01 g of the polymerization agent to benzene and 0.1 mol1H, 1H-pentafluoropropanol were added to the three flasks mounted with a thermometer, a constant pressure drip funnel, and a stirrer, at a temper...
Embodiment 2
[0068] This example is a method of preparing an antibacterial hydrophobic resin comprising the steps of:
[0069] Step 1: 0.06 mol of dichlorosulfoxide, 0.03 g of the polymer polymer added to the three flask mounted with a thermometer, condensate return tube, constant voltage drip funnel, and stirrer, stirring at a temperature of 20 ° C, stirring The mixture was added dropwise on the side of the rate of 300r / min, and the drip rate was 1 drop / s, and the reaction was refluxed under the temperature of 50 ° C, and the reaction product was cooled after the reaction was completed. After room temperature, the fraction of 32 ° C was collected under pressure of 18.7 kPa, resulting in an intermediate 1;
[0070] Step 2: Add 0.03 g of the polymer polymer to the three flask mounted with a thermometer, a constant voltage drip funnel, and a stirrer, and a stirring rate at a temperature of 85 ° C, stirring at a temperature of 85 ° C, stirring rate A 0.1 mol intermediate 1 was added dropwise ...
Embodiment 3
[0077] This embodiment is a method of producing a mask outer packaging bag for a certain time, including the following steps:
[0078] S31: In accordance with the weight, 50 parts of the antibacterial hydrophobic resin from Example 1, 20 copies of butyl acetate, 10 titanium powder, 5 silicon powder, and spare;
[0079] S32: The antibacterial hydrophobic resin, butyl acetate is added to the mixer, and mixed for 30 min under conditions having a stirring rate of 500 r / min to give a mixture;
[0080] S33: Add titanium white powder to the mixture, silicon fine powder continues to stir mixture for 1 h to obtain antibacterial hydrophobic coating;
[0081] S34: 0.1 parts of PBAT20, 60 parts of polylactic acid and 1,4-bis-tert-butyl peroxy isopropylbenzene, and spare;
[0082] S35: Place PBAT, polylactic acid in a vacuum drying tank, dried under temperature of 80 ° C, then dried PBAT, polylactic acid, and crosslinking agent 1,4-bis-t-butyl peroxide Benzene is added to the screw extruder ...
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