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Method for preparing agni electrical contact material based on foaming infiltration process and product thereof

An electrical contact material and infiltration technology, applied in metal processing equipment, contacts, circuits, etc., can solve the problems of low powder strength, skeleton collapse, and inability to form, achieving low body resistance, stable temperature rise, and improved The effect of electric life

Active Publication Date: 2022-08-05
ZHEJIANG FUDA ALLOY MATERIALS TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0011] The Chinese invention patent with the publication number CN104209520A adds a polyacrylate pore-forming agent to the powder to increase the pores. The powder produced by this method has low strength and can meet the production requirements when making AgNi30 and AgNi materials with higher Ni content. When making AgNi materials with a Ni content below 30%, the skeleton will collapse or even burst due to the severe deformation of the pores during the infiltration process.
Similarly, using this method to make high-silver AgNi materials will also have the problem that the skeleton collapses or even bursts during infiltration and cannot be formed.
[0012] The Chinese invention patent with the publication number CN112548099A provides a method for making porous alloy powder by using ammonium bicarbonate foaming agent. The powder made by this method also has the problem that the internal strength of the powder is too low. During the AgNi infiltration process, the powder will cause the skeleton to collapse or even explode due to the severe deformation of the pores, and the mechanism is basically similar to that of the polyacrylate pore-forming agent.

Method used

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  • Method for preparing agni electrical contact material based on foaming infiltration process and product thereof
  • Method for preparing agni electrical contact material based on foaming infiltration process and product thereof
  • Method for preparing agni electrical contact material based on foaming infiltration process and product thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0052] Called 5KG AGNI45 mixed powder, add 5WT % of ammonium carbonate solution, 5WT % ammonium carbonate solution each 500g and stir well. Granules;

[0053] The sieving powder is installed in the graphite boat, transferred to the vacuum oven to heat it to 200 ° C for 60 minutes, and then transfer the foaming powder and graphite boat to the hydrogen atmosphere to burn the sintering and burn 800 ° C for 30 minutes. It

[0054] Mix the sintering powder and heat the powder on the mixer. At the same time, spray 10WT % paraffin-gasoline solution 0.5kg, wrap all the powder, heat up the gasoline in the pink body;

[0055] The powder -loading boats that are wrapped in burn -in -law wrapped in the hydrogen atmosphere for sintering treatment. The sintering process is 400 ° C, 120 minutes, 600 ° C, 120 minutes, 800 ° C, 120 minutes, 1000 ° C, 60 minutes, and the cooling and crushing after sintering have been cooled and crushed. 100 mesh screen, obtain high -strength polychole prefabricated ...

Embodiment 2

[0061] Called 10kg Agni45 mixed powder, add 5WT % dual oxygen solution 1kg and stir well. After the stirred powder sieved with 100 mesh stainless steel to obtain the AGNI powder particles wrapped in the foaming agent;

[0062] The sieving powder is installed in the graphite boat, transferred to the vacuum oven to heated to 60 ° C for 30 minutes, and then transfer the foaming powder and graphite boat to the ammonia decomposition atmosphere of the sintering furnace of 500 ° C, heat preservation 120 120 minute;

[0063] Mix the sintering powder and heat the powder on the mixer. At the same time, spray 1WT % paraffin-gasoline solution 2kg, wrap all the powder, heat the stirring powder in the pink body, dry;

[0064] The powder -loading boats that are wrapped in burn -in -law wrapping are sintering in the atmosphere of ammonia. The sintering process is 500 ° C, 60 minutes, 700 ° C, 60 minutes, 900 ° C, 60 minutes, 1100 ° C, 60 minutes. After 50 mesh screens, obtain a high -strength pol...

Embodiment 3

[0069] Called 5KG AGNI40 mixed powder, add 5WT % ammonium oxalized ammonium oxalate solution, 5WT % ammonium hydrogen ammonium hydrogen ammonium solution and mix well. Granules;

[0070] The sieving powder is installed in the graphite boat, transferred to the vacuum oven to heated to 100 ° C for 60 minutes, and then transfer the foaming powder and graphite boat to the vacuum sintering furnace to burn for 600 ° C for 60 minutes;

[0071] Mix the sintering powder and heat the powder on the mixer. At the same time, spray 4 % paraffin-gasoline solution 0.5kg, wrap all the powder, heat the stirring powder in the pink body;

[0072] The powder -loading boats that are wrapped in burn -in -law wrapped in in the vacuum atmosphere are sintering. The sintering process is 450 ° C, 90 minutes, 650 ° C, 90 minutes, 850 ° C, 90 minutes, 1050 ° C, 90 minutes, and the cooling after sintering is broken and crushed too much too much 80 -mesh screen, obtain high -strength polychide prefabricated AGNI...

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Abstract

The invention discloses a method and a product for preparing AgNi electrical contact materials based on a foaming infiltration process. The technical scheme is that a foaming agent is added to AgNi mixed powder for sintering strengthening, and the sintering-strengthened AgNi powder is wrapped with a separator and sintered Above the liquid phase, it is crushed and sieved to obtain high-strength porous AgNi powder. The porous AgNi powder is isostatically pressed into a special columnar porous skeleton ingot, and then the pure silver sheet is placed above the skeleton and placed in a graphite crucible. The skeleton ingot is infiltrated at high temperature to obtain AgNi / Ag composite ingot with high silver content and low resistivity, and the ingot is extruded into a thin strip and finally punched into AgNi electrical contact material. The invention simultaneously solves the problem of composite extrusion of thin strips and the problem that low-nickel and high-silver AgNi electrical contacts can only be made by solid-phase sintering process. The service life and other performance have been greatly improved.

Description

Technical field [0001] The invention involves the field of electrical contact materials, which specifically refers to a method and its products that prepare an AGNI electrical contact material. This process uses a new foam melting seepage process for preparation. Background technique [0002] The AGNI electrical contact material has many applications in circuit breakers, micro-circuit breakers, leakage protection switches, contactors, and relays. Generally, the sintering sintering method or extrusion method is used. The NI content is between 10WT % -35WT %. The requirements for the switching temperature in the switch design are getting higher and higher, especially in small micro -breaking materials, the Ni content is more than 35WT % of the material contact contact resistance, it is difficult to meet the use requirements, and the electric contact material with low NI content can only be used in solids. The sintering method cannot meet the requirements of switching and short circ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C1/04C22C5/06H01H1/023B22F1/102B22F3/04B22F3/10B22F3/11B22F3/26B22F5/00
CPCC22C1/0466C22C5/06B22F3/1035B22F3/1125B22F3/04B22F3/26B22F5/00H01H1/023
Inventor 林旭彤孔欣费家祥郭仁杰崔永刚宋林云万岱宋振阳刘映飞
Owner ZHEJIANG FUDA ALLOY MATERIALS TECH CO LTD
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