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Method for dyeing green by vegetable dye through one-bath process

A plant dye, green technology, applied in the field of plant dye one-bath dyeing green, can solve the problems of cumbersome modification process of plant dye, poor color fastness of textiles, loss of natural characteristics, etc., to achieve good production quality controllability, color High fastness and wide application range

Pending Publication Date: 2022-03-15
CHINA TEXTILE ACAD JIANGNAN BRANCH
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the Chinese invention patent with the application number 202011087300.X and titled "Green Lyocell fabric dyed with plant dye rosemary and its preparation method", a method of dyeing green with modified rosemary plant dye is disclosed. The method of lyocell, wherein the preparation method of the modified rosemary plant dye is: in the aqueous solution, add rosemary extract, 5wt% formaldehyde aqueous solution and 1-amino-2-sulfate ester synthesized by 3 steps Ethylsulfone ethane is prepared by adjusting the pH with caustic soda solution, reacting at 50-60°C for 30-60 minutes, and then spray-drying. Although the dyeing does not require the addition of mordants, the modification process of plant dyes is cumbersome and uses formaldehyde, Synthetic dye intermediates, contrary to the original intention of using vegetable dyes, make them lose their true natural characteristics
[0006] The second is to first use plant indigo to dye blue, after oxidized water washing, and then over-dye with yellow plant dye to get green: this method can be dyed green in various shades, shades and grayscales, but the process is cumbersome and reproducible. poor
This method has a simple process and good reproducibility, but gardenia blue basically does not dye cellulose fibers, and this method is only suitable for protein fiber textiles such as silk, and the scope of application is narrow; secondly, gardenia yellow is a direct plant dye , the color fastness of the dyed textile is poor

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Method for dyeing green by vegetable dye through one-bath process
  • Method for dyeing green by vegetable dye through one-bath process
  • Method for dyeing green by vegetable dye through one-bath process

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0044] Embodiment 1: one-bath method of the present invention dyes dark green mulberry silk fabric

[0045] (1) Preparation of plant leuco indigo solution: 2500g of soda ash and 2000g of glucose are dissolved in 30L and 10L of water respectively, then 200mL of rice wine, 1000g of cyanine and glucose solution are added to the soda ash solution, and the cyanine is kneaded to make it Reduce and dissolve, stir evenly, and let stand for 30min.

[0046] (2) Preparation of plant indigo leuco acid solution:

[0047] Add 12g of glucose and 600g of natural additives to 4L of water, stir evenly, then slowly add 4L of plant leuco indigo solution into it under high-speed stirring, and stir for 10 minutes under sealed conditions. At this time, the pH value is 5.2.

[0048] Natural aids consist of the following ingredients:

[0049]

[0050] (3) Preparation of color matching vegetable dye solution:

[0051] Add 70g of sumac extract powder, 80g of tea extract powder, 300g of the aforeme...

Embodiment 2

[0060] Embodiment 2: one-bath method of the present invention dyes light green cotton / linen fabric

[0061] (1) Preparation of Plant Leuco Indigo Solution:

[0062] Dissolve 1000g of caustic soda and 1300g of Baowen with 30L and 10L of water respectively, then add 100mL of sorghum wine, 5000g of indigo naturalis, and sodium hydrochloride solution into the caustic soda solution, knead the indigo naturalis to reduce and dissolve, stir evenly, and let it stand for 30 minutes.

[0063] (2) Preparation of plant indigo leuco acid solution:

[0064] Add 8 g of sodium hydrosulfite and 400 g of natural additives into 4 L of water, stir evenly, and slowly add 4 L of plant leuco indigo solution into it under high-speed stirring, and stir for 10 minutes in a sealed manner. At this time, the pH value is 5.0.

[0065] Natural aids consist of the following ingredients:

[0066]

[0067] (3) Preparation of color matching vegetable dye solution:

[0068] Add 200g of pomegranate peel extr...

Embodiment 3

[0077] Embodiment 3: one-bath method dyeing dark green wool of the present invention

[0078] (1) Preparation of Plant Leuco Indigo Solution: Same as Example 1.

[0079] (2) Preparation of plant indigo leuco acid solution: same as in Example 1, 2 L was prepared.

[0080] (3) Preparation of color matching plant dye solution: 30g of yam extract powder, 20g of tea extract powder, 20g of lotus pod extract powder, 30g of natural additives, 2g of glucose, add a small amount of water and stir into a paste, add warm water at about 80°C and stir, After dissolving, add 6g of alum aqueous solution and stir evenly to prepare 1L of color matching plant dye solution.

[0081] (4) Preparation of plant dye green dyeing solution:

[0082] Add the above color-blocking vegetable dye solution into the stirring vegetable indigo leuco acid solution, and mix evenly.

[0083] (5) One-bath green dyeing process of vegetable dyes:

[0084] Immerse 100g of wool fabric in the above dyeing solution, sl...

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Abstract

The invention discloses a method for dyeing green through a vegetable dye one-bath process, and belongs to the technical field of vegetable dye dyeing. Comprising the following steps: preparation of a plant indigo leuco body solution, preparation of a plant indigo leuco acid solution, preparation of a color matching plant dye solution, preparation of a plant dye green dyeing solution, and a plant dye one-bath method green dyeing process. The method for dyeing green by the vegetable dye through the one-bath process is simple in dyeing process, no petrochemical synthetic auxiliary agent is added in the whole process, and the natural and environment-friendly characteristics of vegetable dye are met; the method can be applied to natural fibers such as cotton, hemp, silk, wool and the like or regenerated cellulose fibers and regenerated protein fibers such as viscose, modal, lyocell, soybean protein, milk protein and the like, and is uniform in color, high in color fastness, good in reproducibility, good in production quality controllability and suitable for industrial application.

Description

technical field [0001] The invention relates to a one-bath method for dyeing green with vegetable dyes, and belongs to the technical field of dyeing and finishing in the printing and dyeing industry. Background technique [0002] Vegetable dyes are natural coloring substances extracted from roots, stems, leaves, flowers, fruits, etc. of plants in nature. They are suitable for natural fibers such as silk, wool, cotton, and hemp, or recycled fibers such as Lyocell, Modal, and milk protein fibers. Dyeing of vegan fiber and regenerated protein fiber textiles has the characteristics of wide sources, good compatibility with the environment, biodegradability, and renewable raw materials. It not only has minimal harm to the environment and human body, but also has functional properties, such as anti-oxidation, Antibacterial, anti-ultraviolet, etc., and the color of the dyed fabric is natural, soft and elegant, so it is favored by modern consumers. [0003] my country is one of the ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/34D06P1/22
CPCD06P1/34D06P1/228
Inventor 李俊玲黄逸武严俊杰崔桂新许增慧吕水君黄荣华
Owner CHINA TEXTILE ACAD JIANGNAN BRANCH
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