Moisture-absorption quick-dry antibacterial fabric and preparation method thereof
An antibacterial fabric, moisture-absorbing and quick-drying technology, applied in the field of textiles, can solve problems such as poor moisture absorption and air permeability
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Embodiment 1
[0026] TiO 2 The preparation method of modified polyester comprises the steps:
[0027] (1) Preparation of porous nano-TiO 2 : Add 50g of titanium isopropoxide and 12.5g of dodecyl dimethyl tertiary amine into the reaction flask, mechanically stir evenly, add 1000mL of deionized water, ultrasonically stir, add 7.5g of 30% hydrochloric acid aqueous solution, mechanically stir evenly, heat up to 55°C, keep it warm for 30h, place the filtered residue in an oven, raise the temperature of the oven to 110°C, age for 36h, wash with methanol, and dry in an oven to obtain porous nano TiO 2 ;
[0028] (2) Preparation of TiO 2 Modified polyester: 6g porous nano-TiO 2 , 300g of hydroxyl-terminated polyester, 13.5g of 1,2,3,4-butane tetracarboxylic acid, 9g of acetylacetone, and 2400mL of deionized water were added to the reaction kettle, and mechanically stirred evenly. Continue to heat up to 150°C, keep the temperature for 6 minutes, and get TiO 2 Modified polyester.
Embodiment 2
[0030] TiO 2 The preparation method of modified polyester comprises the steps:
[0031] (1) Preparation of porous nano-TiO 2 : Add 50g of titanium isopropoxide and 18g of dodecyl dimethyl tertiary amine into the reaction flask, mechanically stir evenly, add 1500mL of deionized water, ultrasonically stir, add 15g of 40% hydrochloric acid aqueous solution, mechanically stir evenly, heat up to 60 ℃, heat preservation and rest for 32h, the filter residue obtained by filtration is placed in an oven, the oven is heated to 120°C, aged for 39h, washed with methanol, and dried in an oven to obtain porous nano TiO 2 ;
[0032] (2) Preparation of TiO 2 Modified polyester: 10g porous nano-TiO 2 , 200g of hydroxyl-terminated polyester, 20g of 1,2,3,4-butanetetracarboxylic acid, 12g of acetylacetone, and 2500mL of deionized water were added to the reaction kettle, and mechanically stirred evenly. Continue to heat up to 160°C, keep the temperature for 10 minutes, and get TiO 2 Modified...
Embodiment 3
[0034] TiO 2 The preparation method of modified polyester comprises the steps:
[0035] (1) Preparation of porous nano-TiO 2: Add 50g of titanium isopropoxide and 22.5g of dodecyl dimethyl tertiary amine into the reaction flask, mechanically stir evenly, add 2000mL of deionized water, ultrasonically stir, add 17.5g of 45% hydrochloric acid aqueous solution, mechanically stir evenly, heat up to 65°C, keep it warm for 33h, place the filtered residue in an oven, raise the temperature of the oven to 130°C, age for 42h, wash with methanol, and dry in an oven to obtain porous nano TiO 2 ;
[0036] (2) Preparation of TiO 2 Modified polyester: 12g porous nano-TiO 2 , 200g of hydroxyl-terminated polyester, 28g of 1,2,3,4-butanetetracarboxylic acid, 16g of acetylacetone, and 3000mL of deionized water were added to the reaction kettle, and mechanically stirred evenly. Continue to heat up to 170°C, keep the temperature for 15 minutes, and get TiO 2 Modified polyester.
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