Decorative chromium plating process for imitating stainless steel color
A decorative chrome plating, imitation stainless steel technology, applied in organic chemistry and other directions, can solve the problem of low thickness of chrome layer, and achieve the effect of improving dispersibility, process stability, and appearance without white fog
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preparation example I-1
[0042] An amphoteric pyridinium ligand, prepared by the following method:
[0043] Sa, under nitrogen protection and constant stirring, add 3kg polyethylene glycol to 60kg acetonitrile, then add 5kg1,3,5-tribromomethyl-2,4,6-trimethylbenzene, 6kg ethyl isonicotinate Esters, heated up to 75°C, heat-preserved for 50 hours, filtered, and dried to obtain semi-finished products.
[0044] Sb. Under continuous stirring, add the semi-finished product to 50kg of hydrochloric acid solution, the mass concentration of the hydrochloric acid solution is 20%, heat up to 75°C, heat preservation for 20h, filter, and dry to obtain the amphoteric pyridinium ligand.
preparation example I-2
[0046] An amphoteric pyridinium ligand, the difference between it and Preparation Example I-1 is that the addition of 1,3,5-tribromomethyl-2,4,6-trimethylbenzene is 6kg, isofume The addition of ethyl acetate is 5kg.
preparation example I-3
[0048] An amphoteric pyridinium ligand, the difference between it and Preparation Example I-1 is that 1,3,5-tribromomethyl-2 is replaced with an equal amount of 1,3,5-tribromomethylbenzene, 4,6-Trimethylbenzene.
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