High-strength antistatic 3D sheet and preparation method thereof
An anti-static and high-strength technology, applied in the field of resin sheet processing, can solve the problems of combustion and explosion, breakdown of mobile phone components, loss of mobile phone life and other problems, and achieve the effect of improving service life, improving mechanical strength and improving heat dissipation.
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Embodiment 1
[0053] A high-strength antistatic 3D sheet, the preparation method comprising the following steps;
[0054] (1) Preparation of prepreg: S1. Mix nano-diamond powder and toluene solvent, and ultrasonically disperse for 7 minutes to obtain nano-diamond dispersion; under nitrogen atmosphere, drop nano-diamond dispersion into red aluminum solution, under inert gas protection The temperature was raised to 115 °C, reacted for 4 h, washed with distilled water for three times, dehydrated with a vacuum degree of -0.099MpaMpa, and dried to constant weight to obtain pretreated nano-diamond powder;
[0055] S2 Dissolve modified phenolic resin α in dimethylformamide, cool down to -20°C, add cross-linking agent hydroxyethyl cellulose, antioxidant dibutyl hydroxytoluene, pretreated nano-diamond powder, stir for 8 minutes, and then Add polyamide curing agent, stir for 30min, stirring speed is 800r / min to obtain glue;
[0056] S3. Arrange the glass fibers in the mixed solution of PEDOT and sod...
Embodiment 2
[0065] A high-strength antistatic 3D sheet, the preparation method comprising the following steps;
[0066] (1) Preparation of prepreg; S1. Mix nano-diamond powder and toluene solvent, ultrasonically disperse for 9 min, to obtain nano-diamond dispersion; under nitrogen atmosphere, drop nano-diamond dispersion into red aluminum solution, under inert gas protection The temperature was raised to 127°C, reacted for 5h, washed three times with distilled water, dehydrated with a vacuum degree of -0.097Mpa, and dried to constant weight to obtain pretreated nano-diamond powder;
[0067] S2. Dissolve the modified phenolic resin α in dimethylformamide, cool down to -20°C, add crosslinking agent hydroxyethyl cellulose, antioxidant dibutyl hydroxytoluene, pretreated nano-diamond powder, stir for 9 minutes, Then add polyamide curing agent, stir for 32min, stirring speed is 900r / min to obtain glue;
[0068] S3. Arrange the glass fibers in the mixed solution of PEDOT and sodium polystyrene ...
Embodiment 3
[0077] A high-strength antistatic 3D sheet, the preparation method comprising the following steps;
[0078] (1) Preparation of prepreg: S1. Mix nano-diamond powder and toluene solvent, and ultrasonically disperse for 7 minutes to obtain nano-diamond dispersion; under nitrogen atmosphere, drop nano-diamond dispersion into red aluminum solution, under inert gas protection The temperature was raised to 115 °C, reacted for 4 h, washed with distilled water for three times, dehydrated with a vacuum degree of -0.099MpaMpa, and dried to constant weight to obtain pretreated nano-diamond powder;
[0079] S2 Dissolve modified bisphenol A resin α in dimethylformamide, cool down to -20°C, add cross-linking agent hydroxyethyl cellulose, antioxidant dibutyl hydroxytoluene, pretreated nano-diamond powder, and stir for 8 minutes , then add the polyamide curing agent, stir for 30min, and the stirring speed is 800r / min to obtain the glue;
[0080]S3. Arrange the glass fibers in the mixed soluti...
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