Process for treating industrial waste water from production of furfural
A technology for industrial wastewater and treatment methods, which is applied in the directions of water/sewage multi-stage treatment, heating water/sewage treatment, adsorption water/sewage treatment, etc. It can solve the problems of large investment, high operating cost, instability, etc., and achieve operating costs Low, reduced extraction volume, small footprint effect
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Embodiment 1
[0020] Include the following steps:
[0021] 1. Neutralization of waste water: The waste water at the bottom of the tower produced in furfural production passes through a fluidized bed made of limestone, and the contact time is 1 hour, so that the waste water is neutralized to a pH value of 7;
[0022] 2. Concentration of raffinate: After neutralizing the waste water with a pH value of 7, it enters the double-effect evaporation system to evaporate the water in the waste water, and the raffinate is concentrated. When the solid content of the concentrated liquid is 40%, it is discharged;
[0023] 3. Adsorption filtration: move the raffinate discharged in step 2 into the reaction kettle, add 10% powdered activated carbon by weight, heat to boiling, absorb for 1 hour, centrifuge with a centrifuge at 1800 rpm, and filter;
[0024] 4. Dry the filtrate: dry the filtered liquid in step 3 to separate out white calcium acetate.
Embodiment 2
[0026] Include the following steps:
[0027] 1. Neutralization of waste water: The tower bottom waste water generated in furfural production passes through a fluidized bed made of limestone, and the contact time is 1.2 hours, so that the waste water is neutralized to a pH value of 7.5;
[0028] 2. Concentration of raffinate: After neutralizing the waste water with a pH value of 7.5, it enters the double-effect evaporation system to evaporate the water in the waste water, and the raffinate is concentrated. When the solid content of the concentrated liquid is 40%, it is discharged; the furfural production The aldehyde gas generated at 130°C to 150°C is passed into the double-effect evaporation system as a heat source.
[0029] 3. Adsorption filtration: move the raffinate discharged in step 2 into the reactor, add 12% powdered activated carbon by weight, heat to boiling, absorb for 1 hour, centrifuge with a centrifuge at 1860 rpm, and filter;
[0030] 4. Dry the filtrate: dry th...
Embodiment 3
[0032] In step 2: the water vapor evaporated by the double-effect evaporation system is heat-exchanged through the heat exchanger, and the cooling water is heated to 65°C-75°C as supplementary water for the boiler.
[0033] All the other steps are the same as in Example 1.
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