Silk fiber reinforced high polymer composite material
A technology of silk fiber and composite material is applied in the field of fiber reinforced material and silk fiber reinforced polymer composite material to achieve the effects of improving mechanical properties, good biocompatibility and low price
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Embodiment 1-4
[0012] The mechanical properties of silk fiber reinforced polycaprolactone (PCL) composites with different fiber contents are shown in Table 1. The matrix and fibers with different composition ratios were stirred in a high-speed mixer for 15 minutes to make them evenly mixed, and then mixed in an internal mixer Mix at 140°C for 15 minutes, press with a flat vulcanizer at 140°C for 15 minutes at a pressure of 25 MPa, and then release the mold after cold pressing at room temperature for 10 minutes while keeping the pressure constant. According to the standard of GB1042-79, the mechanical performance test is carried out. It can be seen from Table 1 that with the addition of fibers, the mechanical performance of the composite material has been significantly improved.
Embodiment 5-8
[0014] The mechanical properties of silk fiber-reinforced polylactic acid (PLA) composites with different fiber contents are shown in Table 2. The matrix and fibers with different composition ratios were stirred in a high-speed mixer for 15 minutes to make them evenly mixed, and then mixed in an internal mixer at 140 Mix at ℃ for 15 minutes, press with a flat vulcanizer at 140 ℃ for 15 minutes under a pressure of 25 MPa, and then release the mold after cold pressing at room temperature for 10 minutes while keeping the pressure constant. According to the standard of GB1042-79, the mechanical performance test is carried out. It can be seen from Table 2 that with the addition of fibers, the mechanical performance of the composite material has been significantly improved.
Embodiment 9-10
[0016] A blend of polycaprolactone (PCL) / polylactic acid (PLA) was used as a matrix, the mass ratio of the two in the matrix was changed, and the mass fraction of silk fiber was kept constant. Stir the matrix and fibers in a high-speed mixer for 15 minutes to make them evenly mixed, then knead them in an internal mixer at 140°C for 15 minutes, and mold them with a flat vulcanizer at 140°C for 15 minutes under a pressure of 25MPa, keeping the pressure constant Demould after cold pressing at room temperature for 10 minutes. The mechanical properties were tested according to the standard of GB1042-79, and the specific mechanical properties are shown in Table 3.
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