Magnesium-zine-series ferrite and preparing method
A ferrite and magnesium-zinc technology is applied in the field of preparation of magnesium-zinc ferrites, which can solve the problems of high sintering temperature, poor tin immersion performance at high temperature, and defects in use, and achieves low sintering temperature, low cost, and high compatibility. than reasonable effect
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Embodiment 1
[0022] Shanghai Baosteel Fe 3 o 4 49.8mol%, Zhongsui MgO 24.4mol%, Shanghai Jinghua ZnO25.8mol%, added as the main component, adding 3.4wt% CuO, 0.8% MnCO 3 . The above-mentioned main components and auxiliary components are mixed and ground; pre-fired in an air kiln, the pre-fired holding temperature is 960°C±10°C, and the holding time is 2 hours; the pre-fired powder and binder such as polyvinyl alcohol , dispersant, defoamer and other auxiliary materials are mixed and sand milled, spray granulated, and the average particle size Φ is controlled to be 80 μm to 300 μm; the granular material is pressed into a ring magnetic core of H25mm×15mm×7.5mm, pressed and cut DR8mm ×10mm I-shaped magnetic core. Heat up the above magnetic core gradually in an air kiln, keep it warm at 1100℃±10℃ for 3.5 hours, then gradually cool it down, the magnetic core number is N1.
Embodiment 2
[0024] Shanghai Baosteel Fe 3 o 4 50.5mol%, Zhongsui MgO 23.4mol%, Shanghai Jinghua ZnO 26.1mol%, added as the main component, added 4.1wt% CuO, 0.4% MnCO 3 , adding other subcomponents 0.004wt% Co 2 o 3 , 0.003V 2 o 5 . The above-mentioned main components and auxiliary components are mixed and ground; pre-fired in an air kiln, the pre-fired holding temperature is 940°C±10°C, and the holding time is 2.5 hours; the pre-fired powder and binder such as polyvinyl alcohol , dispersant, defoamer and other auxiliary materials are mixed and sand milled, spray granulated, and the average particle size Φ is controlled to be 80 μm to 300 μm; the granular material is pressed into a ring magnetic core of H25mm×15mm×7.5mm, pressed and cut DR8mm ×10mm I-shaped magnetic core. Raise the temperature of the above magnetic core gradually in an air kiln, keep it warm at 1120°C±10°C for 3 hours, and then gradually cool it down. The magnetic core number is N2.
Embodiment 3
[0026] Shanghai Baosteel Fe 3 o 4 51.3mol%, Zhongsui MgO 24.0mol%, Shanghai Jinghua ZnO 24.7mol%, added as the main component, added 4.1wt% CuO, 0.3% MnCO 3 , adding other subcomponents 0.002wt% Co 2 o 3 , 0.003V 2 o 5. The above-mentioned main components and auxiliary components are mixed and ground; pre-fired in an air kiln, the pre-fired holding temperature is 920°C±10°C, and the holding time is 3 hours; the pre-fired powder and binder such as polyvinyl alcohol , dispersant, defoamer and other auxiliary materials are mixed and sand milled, spray granulated, and the average particle size Φ is controlled to be 80 μm to 300 μm; the granular material is pressed into a ring magnetic core of H25mm×15mm×7.5mm, pressed and cut DR8mm ×10mm I-shaped magnetic core. Raise the temperature of the above magnetic core gradually in an air kiln, keep it warm at 1150°C±10°C for 2.5 hours, and then gradually cool it down. The magnetic core number is N3.
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