Process for producing polyolefin and vapor-phase polymerization apparatus therefor
A technology of olefin polymerization and polyolefin, applied in chemical/physical/physical-chemical process, chemical instrument and method, chemical/physical process, etc., can solve the problems of blocking the discharge pipe of polymer particles, adhesion, etc.
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[0061] Embodiment 1: the production of propylene-ethylene block copolymer
[0062] (1) Production of magnesium compound (a)
[0063] A glass reactor (capacity: about 12 L) equipped with a stirrer was sufficiently purged with nitrogen, and then charged with 4860 g of ethanol, 32 g of iodine and 320 g of metallic magnesium. The contents of the reactor were heated to react with each other while stirring under reflux until no hydrogen gas was generated from the reaction system to obtain a solid reaction product. The solid reaction product thus obtained was dried under reduced pressure to obtain a magnesium compound (a) [solid product].
[0064] (2) Preparation of solid catalyst component (A)
[0065] Into a three-neck glass Erlenmeyer flask (volume: 5 L) which was sufficiently purged with nitrogen gas, 160 g of the above-mentioned unpulverized magnesium compound (a), 80 ml of purified heptane, 24 ml of silicon tetrachloride and 23 ml of diethyl phthalate were charged. ester. W...
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