Method for preparing aluminium iron polychloride floculant
A technology of polyaluminum chloride and iron floc, which is applied in the direction of flocculation/sedimentation water/sewage treatment, etc., to achieve the effects of process innovation, product stability, and consumption saving
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Embodiment 1
[0028] As shown in Figure 1, the preparation of composite inorganic macromolecule flocculant polyaluminum ferric chloride liquid product by using steel mill waste blast furnace gas ash comprises the following steps:
[0029] (1) Raw material selection: the Fe 2 o 3 The content is 24.32%, Al 2 o 3 Steel plant waste blast furnace gas ash with a content of 8.42% is naturally air-dried and passed through a 60-mesh sieve for subsequent use;
[0030] (2) Laboratory preparation of blast furnace gas ash dissolution solution: take 50g blast furnace gas ash, put it into a 500mL four-neck flask with a stirrer, thermometer and reflux device, add 2gNaF, and add 6mL mass percentage concentration while stirring. 49% HNO 3 To oxidize the ferrous iron in the blast furnace gas ash, use a hydrochloric acid solution with a mass percent concentration of 18% at a gray-acid ratio of 1:3 and a reaction temperature of 100-105°C for 3 hours to make the iron in the material , aluminum is dissolved ...
Embodiment 2
[0034] The method for preparing polyaluminum ferric chloride liquid flocculant by using steel mill waste blast furnace gas ash comprises the following steps:
[0035] (1) Raw material selection: the Fe 2 o 3 The content is 21.2%, Al 2 o 3Steel plant waste blast furnace gas ash with a content of 7.8% is passed through a 60-mesh sieve after natural air-drying, and is set aside;
[0036] (2) Laboratory preparation of blast furnace gas ash dissolution solution: take 50g blast furnace gas ash, put it into a 500mL four-neck flask with a stirrer, thermometer and reflux device, add 2gNaF, and add 6mL mass percentage concentration while stirring. 49% HNO 3 To oxidize the ferrous iron in the blast furnace gas ash, use a hydrochloric acid solution with a mass percent concentration of 18% at a gray-acid ratio of 1:4 and a reaction temperature of 70 to 85°C for 2 hours to make the iron in the material , aluminum is dissolved in the liquid phase to the greatest extent, and then suction...
Embodiment 3
[0040] The method for preparing polyaluminum ferric chloride liquid flocculant by using steel mill waste blast furnace gas ash comprises the following steps:
[0041] (1) Raw material selection: the Fe 2 o 3 The content is 25.2%, Al 2 o 3 Steel plant waste blast furnace gas ash with a content of 8.8% is passed through a 60-mesh sieve after natural air-drying, and is set aside;
[0042] (2) Laboratory preparation of blast furnace gas ash dissolution solution: take 50g blast furnace gas ash, put it into a 500mL four-neck flask with a stirrer, thermometer and reflux device, add 2gNaF, and add 6mL mass percentage concentration while stirring. 49% HNO 3 To oxidize the ferrous iron in the blast furnace gas ash, use a hydrochloric acid solution with a mass percent concentration of 18% at a gray-acid ratio of 1:2 and a reaction temperature of 50 to 65°C, and stir for 4 hours to make the iron in the material , aluminum is dissolved in the liquid phase to the greatest extent, and t...
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