Lubricating Oil Composition
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[0097]The present invention is illustrated by the following, non-limiting examples. Examples 1-4 are lubricant compositions made from the components shown in Table 1 using techniques which are well known in the art. The base stock ratio was constant in all of the exemplified compositions.
[0098]Examples 3 and 4 contained an ashless (non-metallized) methylene bridged alkyl phenol having a weight average molecular weight ranging from 1100 to 1700. The ashless methylene bridged alkyl phenol was prepared by adding dodecylphenol, sulphonic acid (catalyst), paraformaldehyde, water and heptane to a 5 L baffled reactor provided with a stirrer (200 rpm), nitrogen blanket (600 ml / min), condenser, Dean and Stark trap, a temperature controlling system, and Cardice / Acetone trap vacuum system. The reaction components were heated from ambient to 80° C. over 30 minutes, then heated further from 80° C. to 100° C. over 2 hours, during which time water was removed by azeotropic distillation. The residu...
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