Method for producing linen glue
A production method and technology for flax glue, applied in chemical instruments and methods, natural resin technology and other directions, can solve the problems of complicated and time-consuming steps, increased solid impurities, low economic added value, etc., and achieve improved application value, high extraction efficiency, and improved The effect of glue purity
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Embodiment 1
[0026] After the high-quality linseeds are selected, cleaned and removed, weigh 20g, add 50ml of 95% ethanol solution with NaOH content of 0.1%, stir and mix at 25°C for 30min, filter, and the filtrate is used to extract lignans, and add 100°C heat to the filter cake Water 50g, blanching for 8min, suction filtration, adding filter cake to 150g water, adjusting water temperature to 40°C, adding 0.1% water weight xylanase, stirring for 1 hour, then adding 0.1% water weight mycoprotein Polysaccharase, stirred for 0.5 hours, suction filtered, collected the filter cake, added 60g of water at 40°C to repeat the extraction once, combined the two extracts to obtain liquid flax gum; concentrated the liquid flax gum, spray-dried to obtain 1.7g of white flax gum powder, The polysaccharide content was determined to be 90%, and the protein content was determined to be 4%.
Embodiment 2
[0028] After the high-quality linseeds are selected, cleaned and removed, weigh 20g, add 50ml of 85% methanol solution with a KOH content of 2.0%, stir and mix at 20°C for 30min, filter, and the filtrate is used to extract lignans, and add 95°C heat to the filter cake Water 20g, blanching for 5min, filtering, adding the filter cake to 100g of water, adjusting the water temperature to 45°C, adding 0.01% water weight xylanase, stirring for 2 hours, then adding 0.01% water weight mycoproteoglycan Enzyme, stirred for 1 hour, filtered with suction, collected the filter cake and added 80g of water at 45°C to repeat the extraction once, combined the two extracts to obtain liquid flax glue; concentrated the liquid flax glue, spray-dried to get 1.5g of white flax glue powder, measured The polysaccharide content is 93%, and the protein content is 5%.
Embodiment 3
[0030] After the high-quality linseed is selected and cleaned and removed, weigh 20g, add Na 2 CO 3 50ml of 90% methanol solution with a content of 5%, stirred and mixed at 50°C for 30min, filtered, the filtrate was used to extract lignans, added 60g of hot water at 90°C to the filter cake, blanched for 10min, filtered, and added to 200g of water , adjust water temperature to be 55 ℃, add the xylanase of 0.5% water weight, stir 1 hour, then add the fungal proteoglycanase of 0.5% water weight, stir 2 hours, press filter, collect filter cake and add 100g water 55 Repeat the extraction once at ℃, and combine the two extracts to obtain liquid flax gum; concentrate the liquid flax gum and dry it with infrared rays to obtain 1.6 g of white flax gum powder, the determined polysaccharide content is 91%, and the measured protein content is 4%.
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