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Method for producing linen glue

A production method and technology for flax glue, applied in chemical instruments and methods, natural resin technology and other directions, can solve the problems of complicated and time-consuming steps, increased solid impurities, low economic added value, etc., and achieve improved application value, high extraction efficiency, and improved The effect of glue purity

Inactive Publication Date: 2007-10-24
SHANXI INST OF COAL CHEM CHINESE ACAD OF SCI +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The disadvantages are: 1. Before the linseed is leached to extract the gum, no effective treatment is carried out, resulting in the extracted flax gum containing pigments such as flavonoids and lignans, which makes the color of the flax gum darker and unstable in nature, directly affecting its quality. It is used in the food industry with higher standards; 2. If the shell and kernel are separated, although the gel extraction rate is increased, it is easy to cause more solid impurities in the glue, which will make the steps such as filtration and centrifugation complicated, time-consuming and inefficient; 3. The method of adding immersion aid (hydrochloric acid or 18-decenoic acid) will also increase the protein content in the product while producing the glue
From the perspective of its drying process, it is not suitable for spray drying production, because sugar and protein are prone to browning at high temperature, resulting in product denaturation, which has adverse effects on product color and viscosity; from the perspective of application prospects, this is not suitable. Bioengineering and pharmaceutical industries that require low protein content
4. The high temperature used in the process of adding the enzyme leaching agent is especially unfavorable for the "active" enzyme, because the enzyme is easily denatured at high temperature
5. The selectivity of flax gum polysaccharide extraction is poor, and the product flax gum contains more components in shell kernels such as protein, lignans, pigments, etc., and the content of flax gum polysaccharides is low; this kind of flax gum is easy to brown
6. Lack of comprehensive utilization considerations, only considering the extraction of rubber, and the high value-added active substances lignans and phytic acid in flaxseed have not been effectively utilized, so the economic added value of its application is low

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] After the high-quality linseeds are selected, cleaned and removed, weigh 20g, add 50ml of 95% ethanol solution with NaOH content of 0.1%, stir and mix at 25°C for 30min, filter, and the filtrate is used to extract lignans, and add 100°C heat to the filter cake Water 50g, blanching for 8min, suction filtration, adding filter cake to 150g water, adjusting water temperature to 40°C, adding 0.1% water weight xylanase, stirring for 1 hour, then adding 0.1% water weight mycoprotein Polysaccharase, stirred for 0.5 hours, suction filtered, collected the filter cake, added 60g of water at 40°C to repeat the extraction once, combined the two extracts to obtain liquid flax gum; concentrated the liquid flax gum, spray-dried to obtain 1.7g of white flax gum powder, The polysaccharide content was determined to be 90%, and the protein content was determined to be 4%.

Embodiment 2

[0028] After the high-quality linseeds are selected, cleaned and removed, weigh 20g, add 50ml of 85% methanol solution with a KOH content of 2.0%, stir and mix at 20°C for 30min, filter, and the filtrate is used to extract lignans, and add 95°C heat to the filter cake Water 20g, blanching for 5min, filtering, adding the filter cake to 100g of water, adjusting the water temperature to 45°C, adding 0.01% water weight xylanase, stirring for 2 hours, then adding 0.01% water weight mycoproteoglycan Enzyme, stirred for 1 hour, filtered with suction, collected the filter cake and added 80g of water at 45°C to repeat the extraction once, combined the two extracts to obtain liquid flax glue; concentrated the liquid flax glue, spray-dried to get 1.5g of white flax glue powder, measured The polysaccharide content is 93%, and the protein content is 5%.

Embodiment 3

[0030] After the high-quality linseed is selected and cleaned and removed, weigh 20g, add Na 2 CO 3 50ml of 90% methanol solution with a content of 5%, stirred and mixed at 50°C for 30min, filtered, the filtrate was used to extract lignans, added 60g of hot water at 90°C to the filter cake, blanched for 10min, filtered, and added to 200g of water , adjust water temperature to be 55 ℃, add the xylanase of 0.5% water weight, stir 1 hour, then add the fungal proteoglycanase of 0.5% water weight, stir 2 hours, press filter, collect filter cake and add 100g water 55 Repeat the extraction once at ℃, and combine the two extracts to obtain liquid flax gum; concentrate the liquid flax gum and dry it with infrared rays to obtain 1.6 g of white flax gum powder, the determined polysaccharide content is 91%, and the measured protein content is 4%.

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PUM

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Abstract

The production process of linen glue with linen seed as material includes the following steps: mixing linen seed with 1.0-10.0 % concentration alkali solution, 85-100 % concentration water solution or 0.1-5.0 % concentration alcohol water solution of alkali at 20-50 deg.c to extract lignin compltetely, filtering, scalding the filter cake with 95-100 deg.c water for 5-15 min, mixing the filter cake with water at 25-55 deg.c, xylanase and mycoprotein polysaccharide enzyme through stirring, filtering, re-extracting the filter cake, merging filtrate, and drying to obtain linen glue. The present invention has high linen glue extracting efficiency, and the linen glue product has linen glue polysaccharide content over 90 wt%, low protein content and no pollutant.

Description

technical field [0001] The invention relates to a method for extracting linseed gum from linseed. technical background [0002] Flaxseed, commonly known as flax, is widely distributed in Inner Mongolia, Gansu, Xinjiang and other places. Flaxseed contains more chemical components such as flax gum, phytic acid, lignans, protein, fatty acids, phenolic acids, flavonoids, carotene, lecithin and vitamins B, C, E and minerals. [0003] Flaxseed gum contained in flaxseed, also known as flaxseed gum, is a polysaccharide-based chemical component. Flax glue is a kind of natural non-polluting vegetable glue. It is a special additive for green food recognized by the National Green Food Development Center. It has high nutritional content, high viscosity, strong water absorption, easy foaming, good emulsification effect, and has adsorption and detoxification effects on heavy metals. . Flax glue is attached to the epidermis of flaxseed, and the general content is 3%-10%. As a dietary fi...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09F1/00
Inventor 侯相林杜俊民邓天昇
Owner SHANXI INST OF COAL CHEM CHINESE ACAD OF SCI
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