Method for preparing nano TiO2 polyester ether elastic fiber
A technology of polyether ester elastomer and elastic fiber, which is applied in the field of preparation of nano-TiO2 polyether ester elastic fiber, to achieve the effects of stable chemical properties, uniform fiber size, and simple process
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Embodiment 1
[0029] Using dimethyl terephthalate (DMT), polytetrahydrofuran ether glycol (PTMO), and 1,4-butanediol (BD) as raw materials, adding nano-TiO with a mass fraction of 0.3% 2 Participate in copolymerization, first vacuumize at 100°C to remove water, then raise the temperature to 200°C for transesterification reaction, the transesterification reaction is considered to be complete when the amount of methanol distilled is about 90% of the theoretical amount; raise the temperature to about 250°C, First remove small liquid molecules under low vacuum conditions, then conduct polycondensation reaction for 3 hours while ensuring that the vacuum degree is less than 80Pa, and finally discharge under nitrogen protection to obtain polyether ester elastomers;
[0030] The above polyether ester elastomer was melt spun at a spinning speed of 1000 m / min to obtain polyether ester elastic fibers. Its elastic recovery rate is more than 97% (100% constant elongation) and more than 84% (300% constan...
Embodiment 2
[0032] Using dimethyl terephthalate (DMT), polytetrahydrofuran ether glycol (PTMO), and 1,4-butanediol (BD) as raw materials, adding nano-TiO with a mass fraction of 0.5% 2 Participate in copolymerization, first vacuumize at 100°C to remove water, then raise the temperature to 200°C for transesterification reaction, the transesterification reaction is considered to be complete when the amount of methanol distilled is about 90% of the theoretical amount; raise the temperature to about 250°C, First remove small liquid molecules under low vacuum conditions, then polycondense for 3.5 hours under the condition of ensuring that the vacuum degree is less than 80Pa, and finally discharge under nitrogen protection to obtain polyether ester elastomers;
[0033] The above polyether ester elastomer was melt spun at a spinning speed of 800 m / min to obtain polyether ester elastic fibers. Its elastic recovery rate is more than 97% (100% constant elongation) and more than 86% (300% constant e...
Embodiment 3
[0035] Using dimethyl terephthalate (DMT), polytetrahydrofuran ether glycol (PTMO), and 1,4-butanediol (BD) as raw materials, adding nano-TiO with a mass fraction of 1.0% 2Participate in copolymerization, first vacuumize at 100°C to remove water, then raise the temperature to 200°C for transesterification reaction, the transesterification reaction is considered to be complete when the amount of methanol distilled is about 90% of the theoretical amount; raise the temperature to about 250°C, First remove small liquid molecules under low vacuum conditions, then polycondense for 4 hours under the condition that the vacuum degree is guaranteed to be less than 80Pa, and finally discharge under nitrogen protection to obtain polyether ester elastomers;
[0036] The above polyether ester elastomer was melt spun at a spinning speed of 1000 m / min to obtain polyether ester elastic fibers. Its elastic recovery rate is more than 97% (100% constant elongation) and more than 88% (300% constan...
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