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86results about "Monocomponent polyetheresters artificial filament" patented technology

Bio-based degradable polyester fiber and preparation method thereof

The invention relates to a bio-based degradable polyester fiber and a preparation method thereof. The preparation method includes: adopting bio-based diol and bio-based binary acid as the raw materials, adopting melt polycondensation, carrying out esterification reaction, segmented pre-polycondensation reaction and final polycondensation reaction successively to obtain bio-based degradable polyester, and then conducting melt spinning forming to obtain the bio-based degradable polyester fiber. Specifically, the segmented pre-polycondensation reaction falls into first pre-polycondensation reaction and second pre-polycondensation reaction, wherein polyethylene glycol is added in the first pre-polycondensation reaction process, and a monomer with a polyhydroxyl structure is added in the secondpre-polycondensation reaction process. The final product has a moisture regain of greater than or equal to 2.0% and a surface contact angle of less than or equal to 60 degrees. The preparation methodprovided by the invention has a simple process, effectively reduces the duration of polycondensation reaction, lowers energy consumption and material consumption, and has good economic benefits. Theproduct prepared by the method provided b the invention has the advantages of good degradability, good fiber mechanical strength and high quality, and has great application prospects.
Owner:DONGHUA UNIV

Preparing method for ordinary-pressure positive-ion dyeable polyester fiber

The invention relates to a preparing method for an ordinary-pressure positive-ion dyeable polyester fiber. The preparing method includes the steps that dimethyl isophthalate-5-sodium benzenesulfonate,ethylene glycol, a catalyst and an anti-ether agent are mixed to be subjected to an ester exchange reaction, the reaction is end, then ethylene glycol and sodium ethylene glycol are added, modulationis carried out, then terephthalic acid, ethylene glycol and a catalyst are mixed, and the mixture is subjected to an esterification reaction; the modulated product after the ester exchange reaction is end and polyethylene glycol are added into an esterification reaction system reaching the end point of the esterification reaction, condensation polymerization is carried out, and spinning melt is obtained; the spinning melt is measured, extruded, cooled, subjected to oil applying, stretched, subjected to heat setting and wound, and the ordinary-pressure positive-ion dyeable polyester fiber is prepared. According to preparing method, generation of impurities in the polyester-fiber production process is reduced, pressure rising of a spinning assembly and a filter is reduced accordingly, the service cycle of the polyester fiber is prolonged, the continuity and the safety of the whole production process are guaranteed, and the preparing method has the good economic value and popularizationvalue.
Owner:JIANGSU HENGKE ADVANCED MATERIALS CO LTD

Preparation method of heat-sensitive copolyester fiber

The invention relates to a preparation method of a heat-sensitive copolyester fiber. The preparation method comprises the following steps: mixing terephthalic acid, aliphatic diol I, a guide and a titanium-silicon-cobalt composite catalyst uniformly, then subjecting the mixture to an esterification reaction, a pre-polycondensation reaction and a final polycondensation in sequence to obtain heat-sensitive copolyester, and then preparing the heat-sensitive copolyester fiber by melt direct spinning; the aliphatic diol I is propylene glycol or butylene glycol; the guide is an ester compound generated by a reaction between dibasic acid and aliphatic diol II; the molar ratio of the terephthalic acid to the aliphatic diol I is 1:(1.05-1.10); the titanium-silicon-cobalt composite catalyst is formed by compounding a titanium-silicon composite catalyst and a cobalt catalyst; the titanium-silicon composite catalyst is obtained by loading a titanium-based catalyst with a silicon-based catalyst; and polysiloxane and a copolymerization component are added during the final polycondensation reaction. The preparation method provide by the invention is few in side reactions and high in reaction rate; an obtained product is concentrated in molecular weight distribution and good in quality; and the fiber is prepared with the melt direct spinning.
Owner:DONGHUA UNIV
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