Preparing method for ordinary-pressure positive-ion dyeable polyester fiber
A polyester fiber, cationic technology, applied in the field of polyester spinning, can solve the problems affecting the continuity and safety of the production process, the rapid rise of the pressure difference of the filter, and the reduction of the service life of the filter, etc., to ensure the spinnability. , the effect of reducing impurities and reducing pressure rise
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Embodiment 1
[0047] A kind of preparation method of atmospheric pressure cationic dyeable polyester fiber, the steps are as follows:
[0048] a) preparing a spinning melt;
[0049] (1) transesterification reaction prepares bishydroxyethyl isophthalate-5-sodium sulfonate;
[0050] First, dimethyl isophthalate-5-sodium benzenesulfonate and ethylene glycol with a molar ratio of 10:1 are put into the preparation kettle, and the catalyst Zn(Ac) is added. 2 Carry out the transesterification reaction at 175°C with the anti-ether agent NaAc until the distilled amount of water reaches 90% of the theoretical value, to obtain bishydroxyethyl isophthalate-5-sodium sulfonate, then add ethylene glycol and Sodium ethylene glycol modulates to obtain the ethylene glycol solution containing 30wt% bishydroxyethyl isophthalate-5-sodium sulfonate, wherein catalyst Zn(Ac) 2 The addition amount is 0.2wt% of the addition amount of dimethyl isophthalate-5-sodium benzenesulfonate, the addition amount of anti-ethe...
Embodiment 2
[0070] A kind of preparation method of atmospheric pressure cationic dyeable polyester fiber, the steps are as follows:
[0071] a) preparing a spinning melt;
[0072] (1) transesterification reaction prepares bishydroxyethyl isophthalate-5-sodium sulfonate;
[0073] First, put dimethyl isophthalate-5-sodium benzenesulfonate and ethylene glycol into the preparation kettle with a molar ratio of 11:1, add the catalyst Zn(Ac) 2 Carry out the transesterification reaction at 178 ℃ after the anti-ether agent NaAc until the distilled amount of water reaches 92% of the theoretical value, and obtain bishydroxyethyl isophthalate-5-sodium sulfonate, then add ethylene glycol and Sodium ethylene glycol modulates to obtain the ethylene glycol solution containing 31wt% bishydroxyethyl isophthalate-5-sodium sulfonate, wherein catalyst Zn(Ac) 2 The addition amount is 0.3wt% of the addition amount of dimethyl isophthalate-5-sodium benzenesulfonate, the addition amount of anti-ether agent NaAc...
Embodiment 3
[0091] A kind of preparation method of atmospheric pressure cationic dyeable polyester fiber, the steps are as follows:
[0092] a) preparing a spinning melt;
[0093] (1) transesterification reaction prepares bishydroxyethyl isophthalate-5-sodium sulfonate;
[0094] First, put dimethyl isophthalate-5-sodium benzenesulfonate and ethylene glycol into the preparation kettle with a molar ratio of 12:1, and add the catalyst Zn(Ac) 2 Carry out the transesterification reaction at 179 ℃ after the anti-ether agent NaAc until the distilled amount of water reaches 91% of the theoretical value, and obtain bishydroxyethyl isophthalate-5-sodium sulfonate, then add ethylene glycol and Sodium ethylene glycol modulates to obtain the ethylene glycol solution containing 32wt% bishydroxyethyl isophthalate-5-sodium sulfonate, wherein the catalyst Zn(Ac) 2 The addition amount is 0.25wt% of the addition amount of dimethyl isophthalate-5-sodium benzene sulfonate, the addition amount of anti-ether ...
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