TaVIn1-xMxSBrF1-yIy:Rez'Ag0.1 optical storage luminescent material and preparation method thereof
A technology of tavin1-xmxsbrf1-yiy and luminescent materials, which is applied in the field of optical storage luminescent materials, can solve problems such as blurred images, unreadable images, and bulky volume, so as to improve the convenience of use, improve luminous performance, and increase the range of flexibility Effect
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Embodiment 1
[0032] Take TaVIn 0.9 Al 0.1 SBrF 0.9 I 0.1 :Eu 0.06 , Au 0.1 As an example, according to the stoichiometric ratio, the TaF 5 , In 2 S 3 , V 2 S 3 , Au 2 S 3 , S, NH 4 F, NH4 Br, NH 4 I, Al 2 o 3 , Eu 2 o 3 Mix and add ethanol to fully grind, then heat the raw material at 60°C for drying; adopt solid state reaction, surround the ground raw material with activated carbon powder and burn for 3 hours in a reducing atmosphere at a high temperature of 800°C. Cool to room temperature; grind the sample and sieve it, wash it twice with ethanol, heat the sample at 60°C for drying; mix the dried sample with methyl methacrylate solution of 1 / 2 the mass of the sample, and dry at 120°C for 2 After hours, grind the sample and sieve it, wash it twice with ethanol, heat the sample at 60°C for drying, and then screen-coat it.
Embodiment 2
[0034] Take TaVIn 0.9 Y 0.1 SBr F 0.9 I 0.1 :Pr 0.04 , Au 0.1 As an example, according to the stoichiometric ratio, the TaF 5 , In 2 S 3 , V 2 S 3 , Au 2 S 3 , S, NH 4 F, NH 4 Br, NH 4 I, Y 2 o 3 , Pr 2 o 3 Mix and add ethanol to fully grind, then heat the raw material at 50°C for drying; use solid-state reaction, surround the ground raw material with activated carbon powder and burn for 3 hours in a reducing atmosphere at a high temperature of 800°C. Cool to room temperature; grind the sample and sieve it, wash it twice with ethanol, heat the sample at 60°C for drying; mix the dried sample with methyl methacrylate solution of 1 / 2 the mass of the sample, and dry at 120°C for 2 After hours, grind the sample and sieve it, wash it twice with ethanol, heat the sample at 60°C for drying, and then screen-coat it.
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