Mg-Ni-(Gd,Nd) bulk amorphous alloy and preparation thereof
A technology of amorphous alloy and bulk, applied in the field of magnesium alloy material and its preparation, Mg-Ni-based bulk amorphous alloy and its preparation, can solve the problem of low formation ability of Mg-Ni-RE based amorphous, resistance Poor corrosion ability, poor plasticity of amorphous alloys, etc., to achieve high amorphous formation ability, good corrosion resistance, and high specific strength
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Embodiment 1
[0025] Embodiment 1, the Mg of diameter 5mm 75 Ni 15 Gd 5 Nd 5 bulk amorphous alloy
[0026] Step 1, according to Mg 75 Ni 15 Gd 5 Nd 5 Raw materials of magnesium, nickel and rare earth gadolinium and neodymium are prepared: Mg, Ni, Gd and Nd metals with a purity greater than 99% and a molar ratio of 75:15:5:5 are used.
[0027] Step 2, vacuumize the electric arc furnace to 3×10 -3 Pa, filled with a pure argon atmosphere with a purity greater than 99.99% to a pressure of 0.5 atm. The arc melting of titanium absorbs oxygen in the atmosphere, and then the raw materials of the first step, gadolinium and neodymium, are repeatedly smelted and purified four times in the electric arc furnace.
[0028] Step 3, vacuumize the electric arc furnace to 3×10 -3 Pa, filled with a pure argon atmosphere with a purity greater than 99.99% to a pressure of 0.5 atm. Arc melting titanium absorbs oxygen in the atmosphere, then mix and melt the gadolinium and neodymium obtained in the seco...
Embodiment 2
[0034] Embodiment 2, the Mg of diameter 3.5mm 75 Ni 15 Gd 7.5 Nd 2.5 bulk amorphous alloy
[0035] Step 1: According to Mg 75 Ni 15 Gd 5 Nd 5Prepare magnesium, nickel and rare earth gadolinium and neodymium raw materials: Mg, Ni, Gd and Nd metals with a purity greater than 99% and a molar ratio of 75:15:7.5:2.5 are used.
[0036] Step 2: Vacuum the electric arc furnace to 3×10 -3 Pa, filled with a pure argon atmosphere with a purity greater than 99.99% to a pressure of 0.5 atm. The arc melting of titanium absorbs oxygen in the atmosphere, and then the raw materials of the first step, gadolinium and neodymium, are repeatedly smelted and purified four times in the electric arc furnace.
[0037] Step 3, vacuumize the electric arc furnace to 3×10 -3 Pa, filled with a pure argon atmosphere with a purity greater than 99.99% to a pressure of 0.5 atm. Arc melting titanium absorbs oxygen in the atmosphere, then mix and melt the gadolinium and neodymium obtained in the second...
Embodiment 3
[0043] Embodiment 3, the Mg of diameter 3.5mm 75 Ni 15 Gd 2.5 Nd 7.5 bulk amorphous alloy
[0044] Step 1: According to Mg 75 Ni 15 Gd 5 Nd 5 Prepare magnesium, nickel and rare earth gadolinium and neodymium raw materials: Mg, Ni, Gd and Nd metals with a purity greater than 99% and a molar ratio of 75:15:2.5:7.5 are used.
[0045] Step 2: Vacuum the electric arc furnace to 3×10 -3 Pa, filled with a pure argon atmosphere with a purity greater than 99.99% to a pressure of 0.5 atm. The arc melting of titanium absorbs oxygen in the atmosphere, and then the raw materials of the first step, gadolinium and neodymium, are repeatedly smelted and purified four times in the electric arc furnace.
[0046] Step 3, vacuumize the electric arc furnace to 3×10 -3 Pa, filled with a pure argon atmosphere with a purity greater than 99.99% to a pressure of 0.5 atm. Arc melting titanium absorbs oxygen in the atmosphere, then mix and melt the gadolinium and neodymium obtained in the secon...
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