High energy ultrasound extraction
A technology of extracting liquid and ultrasonic wave, applied in the field of liquid phase extraction
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[0078] Oak Flavor Extraction
[0079] Use 150ml tap water or 12% ethanol / water or 100% ethanol to extract 40g oak. The sample was stirred (control sample) or sonicated for 10 seconds and 30 seconds, and then the liquid sample was sieved (about 0.8mm mesh), and then filtered with No. 1 Whitman filter paper. The filtrate sub-sample was diluted 3.5 times with water and sent to the Australian Wine Research Institute for oak flavor analysis by GC-MS.
[0080] Result
[0081] The quantitative limit of chemical substances identified by GC-MS (the amount expressed in μg / L in the diluted extract) is guaiacol 3.5, eugenol 35, oak lactone 35, vanillin 35 and furfural 35. Other chemical substances analyzed but below the quantitative limit are: 4-methylguaiacol, 4-ethylphenol, 4-ethylguaiacol and 5-methylguaiacol.
[0082] The extraction data shows that in the same extraction time, compared with the control sample, the use of the above method for ultrasonic treatment can promote the extraction o...
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