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Production method of large-size graphite electrode

A technology of graphite electrode and production method, which is applied in the production field of large-scale graphite electrode to achieve the effects of good electrical conductivity, low resistivity and low thermal expansion coefficient

Inactive Publication Date: 2010-04-21
JIEXIU JUYUAN & COALY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] In order to solve the shortcomings of carbon electrodes caused by various defects in industrial silicon smelting, the invention provides a production method of large-scale graphite electrodes, which solves the problems existing in the current production of graphite electrodes with a diameter greater than 600mm, and can produce ultra-high-power electrodes with a diameter of 960mm. graphite electrode

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0011] Composition ratio (weight ratio): calcined petroleum coke 76%, modified asphalt 24%; the calcined petroleum coke according to the particle size distribution weight percentage: Φ>12mm pellets 4%; Φ8-12mm pellets 10%; Φ4-8mm pellets 15%; Φ2-4mm pellets 13%; Φ≤0.075mm powder 30%; Φ0.075-2mm filler 4%; the coking value of the modified asphalt is above 55%, The softening point is 95-100°C; after the above-mentioned proportions are mixed, it is made by conventional technology, wherein the kneading temperature is 160°C; the paste block size is less than 40mm when the mold is installed.

Embodiment 2

[0013] Composition ratio (weight ratio): 77% of calcined petroleum coke, 23% of modified pitch; the weight percentage of calcined petroleum coke according to particle size distribution is: Φ>12mm pellets 2%; Φ8-12mm pellets 8%; Φ4-8mm pellets 13%; Φ2-4mm pellets 11%; Φ≤0.075mm powder 32%; Φ0.075-2mm filler 11%; the coking value of the modified asphalt is above 55%, The softening point is 95-100°C; after the above-mentioned proportions are mixed, it is made by conventional technology, wherein the kneading temperature is 165°C; the paste lumpiness is less than 40mm when the mold is installed.

Embodiment 3

[0015] Composition ratio (weight ratio): calcined petroleum coke 79%, modified asphalt 21%; the calcined petroleum coke according to the particle size distribution weight percentage: Φ8-12mm pellets 6%; Φ4-8mm pellets 17%; Φ2-4mm particles 9%; Φ≤0.075mm powder 32%; Φ0.075-2mm filler 15%; of which Φ0.5-2mm particle size material 7.5%, Φ0.075-0.5mm material 7.5% . The coking value of the modified asphalt is more than 55%, and the softening point is 95-100°C; after mixing according to the above proportion, it is produced by a conventional process, wherein the kneading temperature is 163°C; the paste lumpiness is less than 40mm during mold loading.

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Abstract

The invention relates to a production method of a large-size graphite electrode which comprises the components in percentage by weight: 76-79 percent of calcined petroleum coke, 21-24 percent of medium-high temperature modified asphalt and the balance of filling material with the diameter of 0.075-2 mm, wherein the calcined petroleum coke comprises the following components in percentage by weight: not more than 4 percent of granules with the diameter of more than 12 mm, 6-10 percent of granules with the diameter of 8-13 mm, 13-17 percent of granules with the diameter of 4-8 mm, 9-13 percent of granules with the diameter of 2-4 mm and 30-32 percent of powder with the diameter of not more than 0.075 mm according to the particle size distribution; and the coking value of the modified asphalt is over 55 percent and the softening point is 95-100 DEG C. After the raw materials are mixed according to the proportion, the large-size graphite electrode is produced by adopting a conventional process, wherein the mixing temperature is 160-165 DEG C and the thicker lumpiness during the die-filling is less than 40 mm. A huge-size electrode with the diameter of over 960 mm can be produced by adopting the production method of the large-size graphite electrode; meanwhile, the electrode has low resistivity and good conduction property and can bear strong current, thereby enabling the unit consumption and the electricity consumption to be greatly lowered and saving the production cost.

Description

Technical field [0001] The invention relates to a production method of electrodes heated by electric discharge, in particular to a production method of graphite electrodes used in electric furnace smelting or industrial silicon electric heating equipment. Background technique [0002] Electrode is a cylindrical object, an important part of industrial silicon smelting electric furnace, and a part of short net. Relying on the electrode to send the low-voltage and large current from the furnace transformer to the furnace, the electric arc at the end of the electrode, the resistance of the charge and the melt, convert the electric energy into heat energy for high-temperature smelting. Therefore, in order to keep the electrode in a sound and stable operating state and minimize the occurrence of electrode accidents, the electrode needs the following requirements: 1) It has good conductivity, moderate resistivity, and matches the electrical parameters to reduce current when passing thro...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/622C04B35/532
Inventor 高峰屹渠果明
Owner JIEXIU JUYUAN & COALY
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