Method for bleaching grey down feather
A down and gray technology, which is applied in the field of down bleaching, can solve the problems of high water bath temperature, incomplete oxidation, easy crushing, etc., and achieve the effect of significantly improving whiteness, less damage to down and down, and improving whiteness
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Embodiment 1
[0021] (1) Pretreatment: configure the pretreatment solution, in which FeSO 4 The concentration is 5% (mass percentage, the same below), the concentration of sodium hypophosphite is 10%, and the pH value of the solution is adjusted to 4 with glacial acetic acid. In the solution, the bath ratio was 1:80, and the temperature was kept for 20 minutes. Take out the down and wash it once with 1g / L sodium hypophosphite solution at 55°C, and then wash it twice with cold water.
[0022] (2) Selective oxidation bleaching: this part is to soak the pretreated down in the oxidation bleaching solution with a pH value of 8-8.5, at 50°C, with a bath ratio of 1:50, and keep warm for 60 minutes, in the oxidation bleaching solution, The concentration of 30% hydrogen peroxide is 30mL / L, and the stabilizer sodium pyrophosphate is 1g / L.
[0023] (3) Thiourea dioxide reductive bleaching: in the reducing bleaching solution, 15 g / L of thiourea dioxide was used, and the down and down after selective ...
Embodiment 2
[0026] (1) Pretreatment: configure the pretreatment solution, in which FeSO 4 The concentration is 40% (mass percentage, the same below), the concentration of sodium hypophosphite is 60%, and then the pH value of the solution is adjusted to 6 with glacial acetic acid. In the solution, the bath ratio is 1:80, keep warm for 50min, take out the down and wash it once with 1g / L sodium hypophosphite solution at 55°C, and then wash it twice with cold water.
[0027] (2) Selective oxidation bleaching: This part is to soak the pretreated down in the oxidation bleaching solution with a pH value of 8-8.5. The concentration of 30% hydrogen peroxide is 60mL / L, and the stabilizer sodium pyrophosphate is 3g / L.
[0028] (3) Thiourea dioxide reduction bleaching: In reduction bleaching solution, thiourea dioxide 25g / L. Place the down and down after selective oxidation bleaching in the reduction bleaching solution with a bath ratio of 1:50, and keep it warm for 20 minutes at a temperature of 5...
Embodiment 3
[0031] (1) Pretreatment: configure the pretreatment solution, in which FeSO 4 The concentration is 15% (mass percentage, the same below), the concentration of sodium hypophosphite is 30%, and the pH value of the solution is adjusted to 5 with glacial acetic acid. In the solution, the bath ratio is 1:80, keep warm for 40min, take out the down and wash it once with 1g / L sodium hypophosphite solution at 55°C, and then wash it twice with cold water.
[0032] (2) Selective oxidation bleaching: this part is to soak the pretreated down in the oxidation bleaching solution with a pH value of 8-8.5. The concentration of 30% hydrogen peroxide is 50mL / L, and the stabilizer sodium pyrophosphate is 2g / L.
[0033] (3) Reductive bleaching with thiourea dioxide: 20 g / L thiourea dioxide in the reducing bleaching solution, place the down and down after selective oxidation bleaching in the reducing bleaching solution with a bath ratio of 1:50, and keep warm for 25 minutes at a temperature of 60°...
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