Multifunctional compound rheological agent and preparation method thereof

A rheological agent and multi-functional technology, applied in the field of preparation of petroleum coke powder-heavy oil-water new fuel system, to achieve the effects of low ignition temperature, complete combustion and lower exhaust gas temperature

Inactive Publication Date: 2012-08-22
山东华材工程检测鉴定有限公司 +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

With the increase in the amount of heavy oil and the gradual shortage of oil, saving petroleum products and improving their application efficiency has become one of the country's important energy-saving content, and a certain amount of petroleum coke powder and water are added to fuel heavy oil to form coke-oil - The new water fuel system has significant economic and social benefits of energy saving and environmental protection. The technical key to formulating this new fuel system is to be able to disperse the three immiscible components evenly, so that it can be pumped and sprayed when applied. And atomization requirements, currently there is no suitable rheology agent with good dispersion, stability, drag reduction (viscosity reduction) function

Method used

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  • Multifunctional compound rheological agent and preparation method thereof
  • Multifunctional compound rheological agent and preparation method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] Embodiment 1, the preparation method of this multifunctional composite rheological agent is:

[0031] A. Preparation of stable rheological agent

[0032] a. Weigh the raw materials according to the mol ratio of each raw material: AM: AA: BS: MA=0.2: 1: 0.03: 0.5, and take kilograms as the unit, AM14.2Kg, AA72Kg, BS6.2Kg, MA49Kg,

[0033] Get the ammonium persulfate of aforementioned raw material gross weight 0.7% that is 0.99Kg as oxygenant,

[0034] Get that 2.12Kg sodium bisulfite of 1.5% of aforementioned raw material gross weight is reducing agent,

[0035] b. Synthesis operation: Add 50% of the total weight of the aforementioned raw materials, that is, 72Kg of water in the reactor to make bottom water and MA, heat to dissolve, add sodium bisulfite and then heat up to 65°C to 70°C, and make the oxidant into 3% The aqueous solution is A drop, and AA+BS+AM is made into a 60% aqueous solution to be B drop. At the same time, A drop and B drop are added dropwise to the...

Embodiment 2

[0037] Embodiment 2, the raw material composition weight and number ratio of stable rheological agent is:

[0038] AM

AAA

BS

MA

21.3

108

0

39.2

28.4

122.4

2.06

58.8

35.5

136.8

4.12

78.4

42.5

144.0

6.18

98.0

[0039] Other ratios in parts by weight of the composite rheological agent are:

[0040]

Embodiment 3

[0041] Embodiment 3, the using method of multifunctional composite rheology agent is: for making tar water slurry according to the weight and number ratio of petroleum coke powder: heavy oil: water=30:60:10, add 1.0% of tar water slurry weight The composite rheological agent is heated to 80°C and stirred for 30 minutes under the condition of a rotating speed of 1500 rpm, and the time for the tar water slurry to be stable without separation is 20 to 25 days.

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Abstract

The invention discloses a multifunctional compound rheological agent and a preparation method thereof, which relate to a rheological agent prepared by unsaturated monomers such as acrylamide and the like through copolyreaction and the preparation method thereof. The compound rheological agent is a composition which is prepared from the products which serve as main components and are obtained by performing the copolyreaction on acrylamide, acrylic acid, styrene sulfonic sodium and maleic anhydride in a certain ratio through an initiating system of oxidation-reduction, and a dispersant and an emulsifier which serve as auxiliaries. The composition is used in used for fuel pulp slurry of petroleum coke powder, heavy oil and water, and has the functions of dispersing and stabilizing a system, and can fulfill the aims of pumpability, spraying capability, atomization, energy conservation and environment protection under use conditions.

Description

technical field [0001] The invention relates to a rheological agent prepared by copolymerization of unsaturated monomers such as acrylamide and its compound preparation method with dispersed and emulsified components, and is mainly used for the preparation of petroleum coke powder-heavy oil-water new fuel system . Background technique [0002] Petroleum is one of the important one-time energy materials. As the heavy oil in petroleum components, it is an important boiler fuel for metallurgy, glass, power generation and other industries. With the increase in the amount of heavy oil and the gradual shortage of oil, saving petroleum products and improving their application efficiency has become one of the country's important energy-saving content, and a certain amount of petroleum coke powder and water are added to fuel heavy oil to form coke-oil - The new water fuel system has significant economic and social benefits of energy saving and environmental protection. The technical...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10L1/24C10L1/236C10L1/198C10L1/19C10L1/32C08F220/06C08F220/56C08F212/08C08F222/08
Inventor 张明征王惠忠梁恩才张锐王美婷
Owner 山东华材工程检测鉴定有限公司
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