Rare-earth doped bismuth titanate up-conversion luminescence nanometer crystal material
A nanocrystalline material, rare earth doping technology, applied in luminescent materials, chemical instruments and methods, etc., can solve the problem of low luminous intensity, and achieve the effect of high luminous intensity, stable performance and low dielectric constant
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specific Embodiment approach 1
[0014] Specific Embodiment 1: In this embodiment, the rare earth-doped bismuth titanate up-conversion luminescent nanocrystalline material is obtained by doping Er into the bismuth titanate matrix through the sol-gel method, and its general formula is (Bi 4(1-x) Er 4x ) Ti 3 o 12 , where x=0.005~0.1.
[0015] The particle size of the rare earth erbium-doped bismuth titanate up-conversion luminescent nanocrystal material in this embodiment is 20-30 nm. The up-conversion luminescent nanocrystalline material of this embodiment emits green light with strong emission intensity under the excitation of a 980nm laser.
[0016] The preparation method of the rare earth erbium-doped bismuth titanate up-conversion luminescent nanocrystalline material of the present embodiment is as follows: 1. Bi(NO 3 ) 3 ·5H 2 O was added to ethylene glycol methyl ether, stirred and dissolved before adding Er(NO 3 ) 3 ·6H 2 O, after stirring and dissolving, drop into tetrabutyl titanate to obtai...
specific Embodiment approach 2
[0017] Embodiment 2: This embodiment differs from Embodiment 1 in that x=0.01˜0.08. Other steps and parameters are the same as those in Embodiment 1.
[0018] The particle size of the rare earth erbium-doped bismuth titanate up-conversion luminescent nanocrystal material in this embodiment is 20-30 nm. The up-conversion luminescent nanocrystalline material of this embodiment emits green light with strong emission intensity under the excitation of a 980nm laser.
specific Embodiment approach 3
[0019] Embodiment 3: This embodiment differs from Embodiment 1 in that x=0.05. Other steps and parameters are the same as those in Embodiment 1.
[0020] The particle size of the rare earth erbium-doped bismuth titanate up-conversion luminescent nanocrystal material in this embodiment is 20-30 nm. The up-conversion luminescent nanocrystalline material of this embodiment emits green light with strong emission intensity under the excitation of a 980nm laser.
[0021] The rare earth erbium-doped bismuth titanate up-conversion luminescent nanocrystalline material in this embodiment is (Bi 3.8 Er 0.2 ) Ti 3 o 12 .
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