Method for synthesizing trans-1,4-cyclohexane diisocyanate
A technology of cyclohexane diisocyanate and cyclohexane dicarboxylic acid, which is applied in the preparation of carboxylic acid nitrogen-containing derivatives, organic chemistry and other directions, can solve the problems of short reaction period and the like, and achieves short reaction period, easy availability of raw materials, and process route. simple effect
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Embodiment 1
[0018] 172.18g trans-1,4-cyclohexanedicarboxylic acid (1mol), 440ml (6mol) thionyl chloride, add in the three-necked flask of reflux condenser, stirring, thermometer and tail gas absorption device, heat and reflux for 4 hours, The excess thionyl chloride was recovered under reduced pressure to obtain 199.5 g of crude trans-1,4-cyclohexanedicarbonyl chloride, with a yield of 94.99%.
Embodiment 2
[0020] 172.18g trans-1,4-cyclohexanedicarboxylic acid (1mol), 440ml (6mol) thionyl chloride, add in the three-necked flask of reflux condenser, stirring, thermometer and tail gas absorption device, heat and reflux for 3.5 hours, The excess thionyl chloride was recovered under reduced pressure to obtain 196.9 g of crude trans-1,4-cyclohexanedicarbonyl chloride, with a yield of 94.21%.
Embodiment 3
[0022] 172.18g trans-1,4-cyclohexanedicarboxylic acid (1mol), 440ml (6mol) thionyl chloride, add in the three-necked flask of reflux condenser, stirring, thermometer and tail gas absorption device, heat and reflux for 3 hours, The excess thionyl chloride was recovered under reduced pressure to obtain 186.7 g of crude trans-1,4-cyclohexanedicarbonyl chloride, with a yield of 89.33%.
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