Single component organic silicon packaging glue cured by ultraviolet for high-power LED
A technology of ultraviolet rays and encapsulation adhesives, applied in adhesives, other chemical processes, chemical instruments and methods, etc., can solve the problems of epoxy resin curing speed, heat resistance, high temperature yellowing, light transmission stability, and heat dissipation that cannot meet performance indicators and other issues, to achieve the effect of improving light transmittance, convenient use, and simple packaging process
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[0055] Synthesis of UV organosilicon encapsulating glue raw material of the present invention
[0056] Component A Synthesis of prepolymers containing acrylate-based polysiloxanes
[0057] Synthesis of A-1 V9
[0058] 1 Raw materials and solvents:
[0059] ①a.w-dihydropolydimethylsiloxane, viscosity (250℃) 2000mm 2 .s -1 Hydrogen content 0.0037% by mass, colorless and transparent, structural formula: V8
[0060] n=about 730 V8
[0061] ②HDDA 1, 6 hexanediol, purchased, purity over 98.5%
[0062] ③Inhibitor: Tris(3.5-di-tert-butyl-4-hydroxybenzyl) isocyanate
[0063] ④ Catalyst: Hexamethyldipyridine diplatinum iodide (solid)
[0064] ⑤ solvent, anhydrous benzene
[0065] 1. Synthesis reaction:
[0066]In the flask, install a stirring temperature medium, a reflux condenser and a dropping cup, and a nitrogen device. Dry first and then flush with nitrogen. Add 4g of HDDA, 800g of anhydrous benzene, 2g of polymerization inhibitor, stir and raise the temperature to 26°C...
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