Method for producing polyglucose

A technology of polydextrose and its production method, which is applied in the field of food additives, can solve problems such as insignificant intestinal peristalsis, low degree of glucose polymerization, poor color, etc., achieve significant molecular weight distribution, prevent and relieve constipation, and solve the effects of wastewater discharge

Inactive Publication Date: 2010-09-08
TIANJIN UNIVERSITY OF SCIENCE AND TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] Based on the above five polydextrose production process patents, their common shortcomings are: complicated process, incomplete or excessive polymerization, low product purity, poor color, etc., and are not suitable for large-scale industrial production
At present, some products in my country contain about 7% monosaccharides and disaccharid

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] A kind of production method of polydextrose, the steps are:

[0025] (1) Edible glucose, sorbitol and other raw materials contain a certain amount of water, which needs to be dried at 100°C for 3 hours until the water content is 4%;

[0026] (2) After glucose, sorbitol and citric acid are deployed according to the weight ratio (80%: 5%: 15%), the raw materials are polymerized at a temperature of 150 ° C, a negative pressure of 0.02 MPa, and a stirring reaction for 3 hours;

[0027] (3) The discharged polymer is added to warm water at 30°C, stirred and dissolved, and then adsorbed and decolorized by XDA-7 homoporous decolorizing resin, after removing negatively charged pigments and macromolecular organic substances with a molecular weight between 200-10000, The polydextrose finished product is obtained by spray drying;

[0028] (4) The polydextrose aqueous solution used for cleaning the reaction tank is prepared and blended to make a polydextrose beverage containing 3%;...

Embodiment 2

[0032] A kind of production method of polydextrose, the steps are:

[0033] (1) Edible glucose, sorbitol and other raw materials contain a certain amount of water, which needs to be dried at 105°C for 3 hours until the water content is 3%;

[0034] (2) After glucose, sorbitol and citric acid are deployed according to the weight ratio (85%: 2%: 13%), the raw materials are polymerized at a temperature of 160 ° C, a negative pressure of 0.04 MPa, and a stirring reaction for 4 hours;

[0035] (3) Add the discharged polymer into warm water at 45°C, stir and dissolve, and then use XDA-7 homoporous decolorization resin to absorb and decolorize, remove negatively charged pigments and macromolecular organic substances with a molecular weight between 200-10000, The finished product is obtained by spray drying;

[0036] (4) The polydextrose aqueous solution used for cleaning the reaction tank is prepared and blended to make a polydextrose beverage containing 4%;

[0037](5) The polydex...

Embodiment 3

[0039] A kind of production method of polydextrose, the steps are:

[0040] (1) Edible glucose, sorbitol and other raw materials contain a certain amount of water, which needs to be dried at 105°C for 4 hours until the water content is 1%;

[0041] (2) After glucose, sorbitol and citric acid are deployed according to the weight ratio (90%: 1%: 9%), the raw materials are polymerized at a temperature of 200 ° C, a negative pressure of 0.06 MPa, and a stirring reaction for 6 hours;

[0042] (3) The discharged polymer is added to warm water at 50°C, stirred and dissolved, and then adsorbed and decolorized by XDA-7 homoporous decolorizing resin, after removing negatively charged pigments and macromolecular organic substances with a molecular weight between 200-10000, The polydextrose finished product is obtained by spray drying;

[0043] (4) The polydextrose aqueous solution used for cleaning the reaction tank is prepared and blended to make a polydextrose beverage containing 5%; ...

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PUM

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Abstract

The invention relates to a method for producing polyglucose, which comprises the following steps: (1) blending glucose, sorbitol and citric acid in a weight percent range of 80-90: 1-5: 9-15, then performing stirring reaction on the mixture for 3 to 8 hours in a reaction kettle at the temperature of between 150 and 200 DEG C under the negative pressure of between 0.02 to 0.06MPa, and performing polymerization reaction on the mixture to obtain a polymer; (2) adsorbing and decoloring the polymer; and (3) spray-drying the polymer to obtain a finished product of the polyglucose. The producing method solves the difficult problems of complex existing production process, incomplete polymerization reaction, low product purity, poor color and luster and the like, and has the advantages of rich raw material source, simple process, high purity of the finished product, adaptability for large-scale industrialized production and the like; and electric heating is adopted during processing, and the water vapor produced in the polymerization reaction is condensed and discharged, so the whole production process reflects the advantages of no waste gas emission, no pollution, little consumed energy, simple process and energy conservation.

Description

technical field [0001] The invention belongs to the field of food additives, and relates to food dietary cellulose, especially a production method of polydextrose. Background technique [0002] Dietary fiber is a nutrient that is not easy to be decomposed by digestive enzymes. It mainly comes from the cell walls of plants and sugars in natural foods. According to the degree of solubility in water, it can be divided into two basic types: water-soluble fiber (poly Glucose) and non-water-soluble fiber, water-soluble fiber is better than non-water-soluble dietary fiber in preventing and treating cardiovascular disease, diabetes, obesity, etc. And the fastest excretion of cholesterol, not only can help control the blood sugar and cholesterol in the blood beyond the optimal level, but also help diabetic patients reduce insulin and triglycerides, which has long attracted the attention of nutritionists, known as "" The seventh nutrient". [0003] Fiber food is known as "the oasis ...

Claims

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Application Information

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IPC IPC(8): C08B37/02A23L1/09A23L1/308A23L29/30A23L33/21
Inventor 王春霞杜连祥路福平任炳善李胜元
Owner TIANJIN UNIVERSITY OF SCIENCE AND TECHNOLOGY
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