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Proportional bio-diesel and preparation method thereof

A biodiesel and blending technology, applied in biofuels, petroleum industry, liquid carbon-containing fuels, etc., can solve the problems of easy deterioration of unsaturated fatty acids, complicated processes, excessive alcohol, etc., and achieve normal atomization, high calorific value, Storage stable effect

Inactive Publication Date: 2010-09-22
郑州侨联生物能源有限公司
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

At present, the chemical transesterification method is mainly used, but the biodiesel synthesis by the chemical transesterification method has the following disadvantages: the process is complicated, the alcohol must be excessive, the subsequent process must have a corresponding alcohol recovery device, the energy consumption is high, the cost is high, and the color is deep. Unsaturated fatty acids are prone to deterioration at high temperatures

Method used

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  • Proportional bio-diesel and preparation method thereof

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Effect test

Embodiment 1

[0020] Mineral diesel oil 45%, vegetable oil 30%, methanol 18%, sodium dodecylsulfonate 2.0%, OP emulsifier 1.5%, triethanolamine 2.0%, naphthenic acid 1.49%, biological compound enzyme 0.01%, the percentage is mass percentage.

[0021] The preparation method is: as shown in the figure, mix vegetable oil with methanol, sodium dodecylsulfonate, OP emulsifier, and triethanolamine according to the above mass percentage; slowly pour the mixed solution into mineral diesel oil while stirring , and at the same time, add naphthenic acid and biological compound enzyme according to the mass percentage requirements, stir and mix thoroughly, and then the -10# blended biodiesel that can be stored for more than half a year without stratification can be obtained.

Embodiment 2

[0023] Mineral diesel 60%, vegetable oil 25%, methanol 10%, sodium dodecylsulfonate 1.0%, OP emulsifier 1.5%, triethanolamine 1.0%, naphthenic acid 1.48%, biological compound enzyme 0.02%, the percentage is mass percentage.

Embodiment 3

[0025] Mineral diesel 60%, vegetable oil 20%, methanol 14%, sodium dodecylsulfonate 1.0%, OP emulsifier 1.5%, triethanolamine 2.0%, naphthenic acid 1.48%, biological compound enzyme 0.02%, the percentage is mass percentage.

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Abstract

The invention discloses a number 10 proportional bio-diesel, which comprises the following substances in percentage by weight: 45 to 60 mineral diesel, 20 to30 plant oil, 10 to 15 methanol, 1.0 to 3.0 naphthenic acid, 1.0 to 3.0 OP emulsifier, 0.8 to 2.0 sodium dodecyl sulfate, 0.5 to 2.0 triethanolamine and 0.01 to 0.03 bio-enzyme. The preparation method comprises the following steps that: the plant oil is uniformly mixed with the methanol, the OP emulsifier, the sodium dodecyl sulfate and the triethanolamine according to the above mass percent, naphthenic acid and bio-enzyme are added to beadequately mixed, and the mixed solution is slowly poured into the mineral diesel under the mixing condition to obtain the number 10 proportional bio-diesel. The proportional bio-diesel has advanced process, environmental protection and stable product performance, is free from liquating grease and methanol after being stored for more than half year at the temperature of minus 10 DEG C, is transparent and stable, and can reach the standard of the number 10 bio-diesel in GB / T20828 - 200 standard. The proportional bio-diesel is proved in the industrial boiler and diesel engine rack test that: the diesel is stable to store and to burn, has high heat value, and is normal to be atomized by oil path and nozzle. The engine is stable to run.

Description

technical field [0001] The invention belongs to the technical field of biodiesel, and mainly relates to a -10# blended biodiesel and a preparation method thereof. Background technique [0002] With the increasingly tense energy supply situation, the research on biodiesel is deepening day by day, and five related methods for preparing biodiesel have been reported successively, namely dilution, microemulsion, pyrolysis, transesterification and biotechnology methods. At present, the chemical transesterification method is mainly used, but the biodiesel synthesis by the chemical transesterification method has the following disadvantages: the process is complicated, the alcohol must be excessive, the subsequent process must have a corresponding alcohol recovery device, the energy consumption is high, the cost is high, and the color is deep. Unsaturated fatty acids are prone to deterioration at high temperatures. In order to solve the above problems, people began to study the synt...

Claims

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Application Information

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IPC IPC(8): C10L1/02C10L1/24C10L1/222C10L1/198C10L1/188C10L1/182
CPCY02E50/13Y02E50/10
Inventor 高永建王洪涛席克忠
Owner 郑州侨联生物能源有限公司
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