R-Fe-B series magnet of gradient resistance and production method thereof
A production method, r-fe-b technology, applied in the direction of magnets, magnetic objects, chemical instruments and methods, etc., can solve the problems of difficulty in applying high-power rotating electrical machines, the magnetic performance of magnets is degraded, etc., to reduce eddy current loss and improve. Efficiency, effect of high magnetic performance
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Embodiment 1
[0027] Raw materials with a purity greater than 99wt% are divided into components (weight percent) (Nd 21 PR 5 Dy 4.5 )Co 2 Cu 0.15 al 0.1 Nb 0.2 B 1 Fe 余量 Prepared, smelted in the vacuum strip billet continuous casting furnace, sent the scales into the hydrogen crushing furnace for hydrogen crushing to obtain hydrogen crushed particles; sent the hydrogen crushed particles into the The jet mill is finely pulverized to obtain a powder A with an average particle size d=3.3 μm, and a part of the powder A is added with 3% Dy with an average particle size d=3.2 μm 2 o 3Powder, mix uniformly to obtain powder B; send powder A and B into the magnetic orientation molding device in an environment with an oxygen content of less than 1%, use a spacer to carry out layered filling along the direction of magnetization, the volume ratio of powder A and powder B It is 3.6:1, and orientation molding is carried out after powder filling; the molded body is sent to a sintering furnace in ...
Embodiment 2
[0034] Raw materials with a purity greater than 99wt% are divided into components (weight percent) (Nd 21 PR 5 Dy 4.5 )Co 2 Cu 0.15 Al 0.1 Nb 0.2 B 1 Fe 余量 Prepared and smelted in a vacuum strip billet continuous casting furnace, the scales are sent to the hydrogen crushing furnace for hydrogen crushing to obtain hydrogen crushed particles; a part of the hydrogen crushed particles are sent to Enter the jet mill for fine pulverization to obtain a powder A with an average particle size d=3.3 μm, and send another part of the crushed particles after hydrogen pulverization into the jet mill for fine pulverization in an environment with an oxygen content of 1.5% to obtain an average particle size d =3.4μm powder B, powders A and B are sent into the magnetic orientation forming device in an environment with an oxygen content of less than 1%, and the spacer plate is used to carry out layered filling along the direction of magnetization, and the volume ratio of powder A to powde...
Embodiment 3
[0036] Raw materials with a purity greater than 99wt% are divided into components (weight percent) (Nd 21 PR 5 Dy 4.5 )Co 2 Cu 0.15 Al 0.1 Nb 0.2 B 1 Fe 余量 , prepared, smelted in a vacuum strip billet continuous casting furnace, sent the scales to the hydrogen crushing furnace for hydrogen crushing to obtain hydrogen crushed particles; the hydrogen crushed particles were sent to Finely pulverize by airflow milling to obtain powder A with an average particle size d=3.3 μm, and add 1% of Al with an average particle size d=1.5 μm to a part of the powder A 2 o 3 Powder, mix uniformly to obtain powder B; send powder A and B into the magnetic orientation molding device in an environment with an oxygen content of less than 1%, use a spacer to carry out layered filling along the direction of magnetization, the volume ratio of powder A and powder B It is 3.6:1, and the powder is filled and then magnetized and formed; the molded body is sent to the sintering furnace in an envir...
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