Process for producing liquid crystal display device
A technology of a liquid crystal display device and a manufacturing method, which is applied in the direction of cable/conductor manufacturing, ion implantation plating, coating, etc., and can solve the problem of lowering the surface resistance of a transparent conductive film, lowering the visual confirmation of a liquid crystal display device, and lowering light transmittance etc. to achieve excellent visual confirmation, high transparency, and low power consumption
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Embodiment 1
[0083] Figure 5 is the H when there is no heating to form a film 2 Curve of the effect of O gas (water vapour). Figure 5 In , A represents the transmittance of the zinc oxide-based transparent conductive film when no reactive gas is introduced. Figure 5In, B stands for H 2 The partial pressure of O gas reaches 5×10 -5 Torr's way only imports H 2 The transmittance of the zinc oxide-based transparent conductive film in the presence of O gas. Figure 5 In, C stands for O 2 The partial pressure of gas reaches 1×10 -5 Torr's way only imports O 2 The transmittance of the zinc oxide-based transparent conductive film in air. As the cathode, a parallel plate type cathode to which a direct current (DC) voltage is applied was used.
[0084] When no reactive gas was introduced, the film thickness of the transparent conductive film was 207.9 nm, and the resistivity was 1576 μΩcm.
[0085] When importing only H 2 In the case of O gas, the film thickness of the transparent cond...
Embodiment 2
[0091] Figure 6 is the H when the substrate temperature is 250°C and the film is formed by heating 2 Curve for the effect of O gas (water vapour). Figure 6 In , A represents the transmittance of the zinc oxide-based transparent conductive film when no reactive gas is introduced. Figure 6 In, B stands for H 2 The partial pressure of O gas reaches 5×10 -5 Torr's way only imports H 2 The transmittance of the zinc oxide-based transparent conductive film in the presence of O gas. Figure 6 In, C stands for O 2 The partial pressure of gas reaches 1×10 -5 Torr's way only imports O 2 The transmittance of the zinc oxide-based transparent conductive film in air. As the cathode, a parallel plate type cathode to which a direct current (DC) voltage is applied was used.
[0092] When no reactive gas was introduced, the film thickness of the transparent conductive film was 201.6 nm, and the resistivity was 766 μΩcm.
[0093] When importing only H 2 In the case of O gas, the fil...
Embodiment 3
[0097] Figure 7 It means that for the heating film formation with the substrate temperature set at 250°C, H is introduced at the same time 2 Gas and O 2 The curve of the effect of gas time. Figure 7 In, A means H 2 The partial pressure of gas reaches 15×10 -5 Torr, O 2 The partial pressure of gas reaches 1×10 -5 The Torr method, the transmittance of the zinc oxide-based transparent conductive film when two gases are simultaneously introduced. Figure 7 Among them, B means O 2 The partial pressure of gas reaches 1×10 -5 Torr's way only imports O 2 The transmittance of the zinc oxide-based transparent conductive film in air. As the cathode, a parallel plate type cathode in which a direct current (DC) voltage and a high frequency (RF) voltage can be superimposed is used.
[0098] While importing H 2 Gas and O 2 In the case of air, the film thickness of the transparent conductive film was 211.1 nm.
[0099] In import only O 2 In the case of air, the film thickness ...
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