Fire coal dust suppressant and preparation method thereof
A dust suppressant, coal-burning technology, applied in chemical instruments and methods, other chemical processes, etc., can solve the problems of poor anti-evaporation ability, short effective dust suppression time, large water consumption, etc. Good dust effect, easy to spray effect
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Embodiment 1
[0041] Prepare coal-fired dust suppressant according to the following steps:
[0042] The first step: in a dry nitrogen environment, add 100 parts of polyether diols with a molecular weight of 1000, 100 parts of polyether diols with a molecular weight of 2000, 80 parts of isophorone diisocyanate, 20 parts of epoxy resin E-51, then add 5 parts of dibutyltin dilaurate T-12, mix well and then heat up to 80°C for 1.5 hours;
[0043] The second step: add 10 parts of 2,2-dimethylolpropionic acid into the three-necked flask, and react at 80°C for 0.5 hours;
[0044] The third step: add 3 parts of diethylene glycol and acetone whose weight is 1 times of the reactant obtained in the second step to the three-necked flask, and react at 50°C for 1.5 hours. polymer, the prepolymer is poured out of the reactor;
[0045] Step 4: Add 3 parts of triethylamine and 200 parts of deionized water to the prepolymer, and stir with a mixer at a rate of 1800 rpm for 10 hours at room temperature to ob...
Embodiment 2
[0048] Prepare coal-fired dust suppressant according to the following steps:
[0049] The first step: under the environment of dry nitrogen, add 200 parts of polyether diols with a molecular weight of 1000, 200 parts of polyether diols with a molecular weight of 2000, 100 parts of isophorone diisocyanate, 35 parts of epoxy resin E-51, then add 15 parts of dibutyltin dilaurate T-12, mix well and then heat up to 90°C for 2.5 hours;
[0050] The second step: add 20 parts of 2,2-dimethylolpropionic acid to the three-necked flask, and react at 90°C for 1.5 hours;
[0051] Step 3: Add 10 parts of diethylene glycol and acetone twice the weight of the reactant obtained in the second step to the three-necked flask, and react at 70°C for 2.5 hours. After the reaction is completed, let it stand until the temperature is 45°C. polymer, the prepolymer is poured out of the reactor;
[0052] Step 4: Add 10 parts of triethylamine and 300 parts of deionized water to the prepolymer, and stir w...
Embodiment 3
[0055]The first step: in a dry nitrogen environment, add 150 parts of polyether diols with a molecular weight of 1000, 150 parts of polyether diols with a molecular weight of 2000, 90 parts of isophorone diisocyanate, 28 parts of epoxy resin E-51, then add 10 parts of dibutyltin dilaurate T-12, mix evenly and heat up to 85°C for 2 hours;
[0056] The second step: add 15 parts of 2,2-dimethylolpropionic acid to the three-necked flask, and react at 85°C for 1 hour;
[0057] The third step: add 5 parts of diethylene glycol and acetone whose weight is 1.2 times the weight of the reactant obtained in the second step to the three-necked flask, and react at 60°C for 2 hours. After the reaction is completed, let it stand until the temperature is 40°C. polymer, the prepolymer is poured out of the reactor;
[0058] Step 4: Add 5 parts of triethylamine and 280 parts of deionized water to the prepolymer, and stir with a mixer at a rate of 1500 rpm for 15 hours at room temperature to obta...
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