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Nano-titanium nitride PEN fiber and preparation method thereof

A nano-titanium nitride and fiber technology, applied in the field of PEN fibers, can solve the problems of no nano-titanium nitride PEN fibers, poor comfort function, poor hygroscopicity of fabrics, etc., to achieve permanent protection against bacterial erosion, excellent washability, Good antibacterial effect

Inactive Publication Date: 2011-05-04
翟育明
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] Chinese patent publication number CN1818170 discloses titanium nitride polyester fiber / cross-section PEN fiber blended yarn and a manufacturing method, wherein the blending ratio of titanium nitride polyester fiber and cross-section PEN fiber is 60-40%; the steps of the product manufacturing method Yes: (1) Use titanium nitride polyester fiber purchased by Liaoyang Petrochemical Co., Ltd., with a single fiber linear density of 1-3D; (2) Use 60-40% cross-section PEN fiber and titanium nitride polyester fiber Blending, the cross-section PEN fiber adopts the cross-section PEN fiber developed by Donghua University, the single fiber linear density is 1-3D, and finally forms a blended yarn; it mainly solves the existing fabrics made of pure titanium nitride polyester fiber , the fabric has poor hygroscopicity, not soft to the touch, poor comfort function, and the technical problem of the glass-like smoothness of the fabric surface, which is suitable for sportswear or summer clothes under the condition where the human body sweats a lot
[0011] At present, there are no reports of functional PEN fibers using nano-titanium nitride as an antibacterial agent

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] (1) Raw material formula of nano titanium nitride PEN masterbatch

[0035] A kind of nano titanium nitride PEN masterbatch, its component mass percentage is,

[0036] Nano titanium nitride 1%

[0037] Compatibilizer 0.1%

[0038] PEN slices 98.9%

[0039] The compatibilizer is white oil;

[0040] The particle size of the nano titanium nitride is 20nm-30nm;

[0041] (2) Preparation method of nano titanium nitride PEN masterbatch

[0042] A kind of nano titanium nitride PEN masterbatch, the raw materials of which are melt blended according to the above mass percentage, the temperature is 250-300℃, the speed is 230-280 rpm, the time is 10-50h, and the nano-nitride is made Titanium PEN masterbatch;

[0043] (3) Raw material composition of nano titanium nitride PEN fiber

[0044] A kind of nano titanium nitride PEN fiber, its component mass percentage is,

[0045] Antibacterial slice masterbatch 1%

[0046] PEN slice 99%

[0047] (4) Preparation method of nano titanium nitride PEN fiber

[00...

Embodiment 2

[0050] (1) Raw material formula of nano titanium nitride PEN masterbatch

[0051] A kind of nano titanium nitride PEN masterbatch, its component mass percentage is,

[0052] Nano titanium nitride 3%

[0053] Compatibilizer 0.2%

[0054] PEN slice 96.8%

[0055] The compatibilizer is white oil;

[0056] The particle size of the nano titanium nitride is 30nm-40nm;

[0057] (2) Preparation method of nano titanium nitride PEN masterbatch

[0058] Same as the preparation method of Example 1 (2).

[0059] (3) Raw material composition of nano titanium nitride PEN fiber

[0060] A kind of nano titanium nitride PEN fiber, its component mass percentage is,

[0061] Antibacterial slice masterbatch 3%

[0062] PEN slice 97%

[0063] (4) Preparation method of nano titanium nitride PEN fiber

[0064] The preparation method is the same as that of Example 1 (4).

Embodiment 3

[0066] (1) Raw material formula of nano titanium nitride PEN masterbatch

[0067] A kind of nano titanium nitride PEN masterbatch, its component mass percentage is,

[0068] Nano titanium nitride 5%

[0069] Compatibilizer 0.5%

[0070] PEN slices 94.5%

[0071] The compatibilizer is white oil;

[0072] The particle size of the nano titanium nitride is 40nm-60nm;

[0073] (2) Preparation method of nano titanium nitride PEN masterbatch

[0074] Same as the preparation method of (2) in Example 1;

[0075] (3) Raw material composition of nano titanium nitride PEN fiber

[0076] A kind of nano titanium nitride PEN fiber, its component mass percentage is,

[0077] Antibacterial slice masterbatch 5%

[0078] PEN slice 95%

[0079] (4) Preparation method of nano titanium nitride PEN fiber

[0080] The preparation method is the same as that of Example 1 (4).

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Abstract

The present invention relates to a nano-titanium nitride PEN fiber and preparation method thereof. The raw material comprises the following components, by mass, 1%-10% of antibacterial masterbatch chips and 90%-99% of PEN chips. The preparation method comprises mixing the antibacterial masterbatch chips with the PEN chips uniformly and performing the melt spinning process to obtain the product. The preparation method is characterized in that the spinning temperature is 260 DEG C - 320 DEG C; the air cooling temperature is 15 DEG C - 25 DEG C; the wind speed is 0.1 m / s - 5 m / s; and the drafting speed is 1500 m / min - 2000 m / min. The nano-titanium nitride PEN fiber of the invention has good antibacterial effect and high safety to human and environment, and can be widely applied.

Description

【Technical Field】 [0001] The invention relates to the technical field of PEN fibers, in particular to a nano titanium nitride PEN (polytrimethylene terephthalate) fiber and a preparation method thereof. 【Background technique】 [0002] Bamboo is an important forest resource in our country. It grows fast, can become a material in a short time, has strong regeneration ability, a successful afforestation, and sustainable felling and utilization. In the past, bamboo was mainly used to make farm tools, fuels, furniture, daily necessities, handicrafts, building materials, flooring, and papermaking, with low utilization value. [0003] With the development of science and technology, the domestic use of bamboo to make bamboo charcoal has greatly expanded its application fields. Because titanium nitride has a special structure, its molecular structure is hexagonal, with dense carbon, large specific gravity, many pores, and rich mineral content. It contains potassium, magnesium, iron, mangan...

Claims

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Application Information

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IPC IPC(8): D01F6/92D01F1/10D01D5/10
Inventor 翟育明
Owner 翟育明