Electric contact material made of silver-tungsten carbide graphite and preparation method thereof
A tungsten carbide graphite, contact material technology, applied in the direction of contacts, electrical components, electrical switches, etc., can solve the problem of difficult to meet the high reliability and electromagnetic compatibility requirements of the fourth-generation low-voltage electrical appliances, anti-oxidation, anti-welding Problems such as poor resistance to arc burning and limiting the application field of contact materials to achieve the effects of high reliability, high electrical life, and high temperature oxidation resistance
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Embodiment 1
[0022] Example 1 , Refer to figure 1 Take the preparation of AgWC9.6ZrC2.4C3 with a size of 7.5×7.5×2.5mm as an example.
[0023] (1) The Ag powder, tungsten carbide-zirconium carbide solid solution and graphite are wet mixed with 0.3% Ni and 0.7% B in a ratio of 85:12:3 for 6 hours, with a ball-to-battery ratio of 1:1, and vacuum drying. Agglomerate and granulate in a hydrogen atmosphere at 700°C for 4 hours to obtain a mixed powder with good fluidity, in which the ratio of tungsten carbide to zirconium carbide in the tungsten carbide-zirconium carbide solid solution is 8:2;
[0024] (2) Press the granulated mixed powder into a 7.5×7.5×3.5mm compact with an initial pressure of 150MPa;
[0025] (3) The compact is sintered in a hydrogen atmosphere at 880°C for 4 hours;
[0026] (4) Recompress the sintered body at a pressure of 250MPa, and the thickness of the green body is 2.8mm;
[0027] (5) Anneal the body after re-pressing in a hydrogen atmosphere at 500°C for 2 hours;
[0028] (6) R...
Embodiment 2
[0031] Example 2 Take the preparation of AgWC9.8ZrC4.2C2 with a specification of 6×6×2mm as an example.
[0032] (1) The Ag powder, tungsten carbide-zirconium carbide solid solution and graphite were wet mixed with 0.4% Cr in a ratio of 84:14:2 for 4 hours, with a ball-to-material ratio of 3:1, dried in a vacuum, and in a hydrogen atmosphere Perform agglomeration granulation at 750°C for 3 hours to obtain a mixed powder with good fluidity, in which the ratio of tungsten carbide to zirconium carbide in the tungsten carbide-zirconium carbide solid solution is 7:3;
[0033] (2) Press the granulated mixed powder into a 6×6×2.8mm compact with an initial pressure of 180MPa.
[0034] (3) The compact is sintered in a hydrogen atmosphere at 900°C for 3 hours;
[0035] (4) Recompress the sintered body at a pressure of 280MPa, and the thickness of the green body is 2.2mm;
[0036] (5) Anneal the body after re-pressing in a hydrogen atmosphere at 600°C for 4 hours;
[0037] (6) Recompress the anne...
Embodiment 3
[0040] Example 3 Take the preparation of AgWC10.8ZrC1.2C3 with a size of 11×9×2mm as an example.
[0041] (1) The Ag powder, tungsten carbide-zirconium carbide solid solution and graphite are wet mixed with 0.3% Ni and 0.7% B in a ratio of 85:12:3 for 6 hours, with a ball-to-battery ratio of 1:1, and vacuum drying. Agglomerate and granulate in a hydrogen atmosphere at 700°C for 4 hours to obtain a mixed powder with good fluidity, in which the ratio of tungsten carbide to zirconium carbide in the tungsten carbide-zirconium carbide solid solution is 9:1;
[0042] (2) Press the granulated mixed powder into a 11×9×2.8mm compact with an initial pressure of 150MPa;
[0043] (3) Sinter the compact in a hydrogen atmosphere at 880°C for 4 hours;
[0044] (4) Re-press the sintered body at a pressure of 250 MPa, and the thickness of the green body is 2.2 mm;
[0045] (5) Anneal the body after re-pressing in a hydrogen atmosphere at 500°C for 2 hours;
[0046] (6) Recompress the annealed body at a...
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