Modifier for polyester enamelled wire insulating paint, and preparation method and application thereof
A manufacturing method and technology of insulating paint, applied in polyester coatings, coatings, etc., can solve the problems of low temperature resistance, increased paint cost, poor thermal shock resistance, etc., and achieve low cost, improved heat resistance and viscosity. The effect of connection performance
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0019] Reactor: a stainless steel stirred reactor with a jacket and an inner coil that can pass through a heating or cooling medium, and is equipped with a vertical fractionator, a horizontal condenser, and a distillate receiving tank. Below the reaction kettle, a dilution kettle is set, and the basic structure of the dilution kettle is a stainless steel stirring reaction kettle with a cooling water jacket.
[0020] Raw materials are charged in molar ratio: the ratio of dibasic acid, tribasic acid and dibasic alcohol is 1:0.05:0.99.
[0021] Weigh 83kg of terephthalic acid, 4.8kg of trimellitic anhydride, 30.8kg of ethylene glycol, and 12g of catalyst zinc acetate into the above-mentioned 300-liter reactor, start the stirrer, heat up to 160°C, fill with nitrogen, and pressurize Under the condition of 0.3MPa (gauge pressure), raise the temperature to 240°C at a constant speed for about four hours, remove the pressure, make the system heat up at a rate of 8-12°C per hour under n...
Embodiment 2
[0024] The reactor was the same as in Example 1.
[0025] Raw materials are charged in molar ratio: the ratio of dibasic acid, tribasic acid and dibasic alcohol is 1:0.2:1.05.
[0026] Weigh 66.4kg of isophthalic acid, 15.4kg of trimellitic anhydride, 44.6kg of diethylene glycol, and 101g of catalyst tetraisopropyl titanate into a 300-liter reactor, start the stirrer, and heat up to 160°C , filled with nitrogen, under normal pressure, after about four hours, the temperature was raised to 240°C at a constant speed, and the system was continued to be heated at a rate of 8-12°C per hour under normal pressure, and the temperature was raised to 265°C, kept warm and sampled to determine the acidity. value, when the acid value drops to 60mg / g, start to cool down, when the temperature drops to 160°C, add 75.8kg of tri-mixed cresols, keep stirring, for about 40 minutes, the temperature drops to 135°C, open the bottom valve of the reaction kettle, and The material was put into a 500-li...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com