3 results about "Mixed cresols" patented technology

The application belongs to the technical field of chemical industry, and particularly relates to a mixed cresol separation method, which comprises selective oxidation, filtration, neutralization, secondary filtration and rectification processes in sequence. The selective oxidation comprises: adding mixed cresol, sodium hydroxide, sodium methoxide, a solvent and a catalyst into an oxidation kettle, heating, and introducing oxygen for selective oxidation. In the selective oxidation step, sodium methoxide is added, which can react with water obtained in a salification reaction step (i.e. a reaction step of sodium hydroxide and mixed cresol to generate sodium phenate and water) to generate methanol and sodium hydroxide, thereby promoting the selective oxidation reaction and improving the yield.

The application discloses a kind of for mixed cresol separation continuous amplification production process and method, belong to mixed cresol separation and purification field.This process solves the problem of low flow, difficult to control, temperature-resistant equipment selection difficult in early stage working condition exploration, proposes the design concept of "breathing mouth".Further, a kind of "exogenous" online detection system can effectively avoid the influence of analysis results due to excessive flow temperature, excessive pressure, high concentration, reduce the complexity of structure design;For the problem of large amount of desorbent, an efficient desorbent extraction system is proposed, which can realize efficient recovery of desorbent and separation and purification of m-cresol product.The process and method are scientific and reasonable, and can realize continuous production, and have important role in mixed cresol separation amplification production.At the same time, it also has wide applicability in other chemical amplification production, separation and purification fields.

The application discloses a mixed cresol type benzoxazine and a preparation method thereof. All materials are heated and sprayed into a reaction container in a mist state, so that the materials are mixed and preliminarily reacted before gathering at the bottom of the reaction container, the mixed cresol type benzoxazine generated in the reaction is prevented from affecting the reaction between unreacted materials in the reaction system too early, and the yield of the mixed cresol type benzoxazine is improved.