Modifying and dyeing method for polyamide textile by using tetrabutyl titanate and reactive dye

A technology of tetrabutyl titanate and reactive dyes, which is applied in dyeing methods, textiles and papermaking, fiber types, etc., can solve the problem that nano-titanium dioxide loading and dyeing cannot be realized simultaneously, nylon fabrics have low anti-ultraviolet and antibacterial properties, and fabric handles and poor air permeability, to achieve the effects of excellent color fastness to sunlight, saving raw materials, and high dyeing percentage

Inactive Publication Date: 2013-04-03
福建金苑服饰有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The purpose of the present invention is to provide a method for modifying and dyeing nylon fabrics by using tetrabutyl titanate and reactive dyes, which solves the problem that the nylon fabrics obtained by the existing modification methods have low anti-ultraviolet and antibacterial properties and long-lasting washing resistance. , nano-titanium dioxide loading and dyeing can not be achieved simultaneously, dyed fabrics have poor level dyeing, poor fabric feel and air permeability, etc.

Method used

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  • Modifying and dyeing method for polyamide textile by using tetrabutyl titanate and reactive dye
  • Modifying and dyeing method for polyamide textile by using tetrabutyl titanate and reactive dye
  • Modifying and dyeing method for polyamide textile by using tetrabutyl titanate and reactive dye

Examples

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Effect test

Embodiment 1

[0028] Weigh 5g of nylon fabric and tetrabutyl titanate respectively, and weigh reactive brilliant blue X-BR dye according to 0.3% of the mass of nylon fabric, wherein the volume ratio of nylon fabric is 1:1 with deionized water and 95% anhydrous Ethanol solution, under the conditions of temperature 80°C, frequency 50KHz, power 100W, ultrasonic vibration washing for 30min, and drying at 60°C. Tetrabutyl titanate was dissolved in deionized water at a ratio of 1:80, reactive brilliant blue X-BR dye was added, and the nylon fabric was immersed in the mixed solution of tetrabutyl titanate dye for 10 minutes, and then the nylon fabric was mixed with titanium Add the aqueous solution of tetrabutyl acid dye to a 200ml high-temperature and high-pressure reactor, fill it with deionized water to 60% of the volume of the reactor, adjust the pH value to 6 with acetic acid, and keep the sealed reactor at 110°C for 6 hours. . After the reaction is over, wash with 2g / L soap flakes and 2g / L ...

Embodiment 2

[0031] Weigh 15g of nylon fabric and 5g of tetrabutyl titanate respectively, and weigh reactive brilliant blue X-BR dye according to 2% of the quality of nylon fabric, wherein the volume ratio of nylon fabric is 1:1 with deionized water and 95% Absolute ethanol solution, under the conditions of temperature 80°C, frequency 50KHz, power 100W, ultrasonic vibration washing for 30min, and drying at 60°C. Tetrabutyl titanate was dissolved in deionized water at a ratio of 1:120, reactive brilliant blue X-BR dye was added, and the nylon fabric was immersed in the mixed solution of tetrabutyl titanate dye for 5 minutes, and then the nylon fabric was mixed with titanium Add the aqueous solution of tetrabutyl ester dye to a 200ml high-temperature and high-pressure reactor, fill it with deionized water to 80% of the volume of the reactor, adjust the pH value to 4 with acetic acid, and keep the sealed reactor at 140°C for 3 hours. . After the reaction is over, wash with 2g / L soap flakes a...

Embodiment 3

[0034] Weigh 10g of nylon fabric and 5g of tetrabutyl titanate respectively, and weigh reactive brilliant blue X-BR dye according to 1% of the mass of nylon fabric, wherein the volume ratio of nylon fabric is 1:1 with deionized water and 95% Absolute ethanol solution, under the conditions of temperature 80°C, frequency 50KHz, power 100W, ultrasonic vibration washing for 30min, and drying at 60°C. Tetrabutyl titanate was dissolved in deionized water at a ratio of 1:100, reactive brilliant blue X-BR dye was added, and the nylon fabric was immersed in the mixed solution of tetrabutyl titanate dye for 8 minutes, and then the nylon fabric was mixed with titanium Add the aqueous solution of tetrabutyl ester dye to a 200ml high-temperature and high-pressure reactor, fill it with deionized water to 70% of the volume of the reactor, adjust the pH value to 5 with acetic acid, and keep the sealed reactor at 120°C for 5 hours. . After the reaction is over, wash with 2g / L soap flakes and ...

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Abstract

The invention discloses a modifying and dyeing method for a polyamide textile by using tetrabutyl titanate and reactive dye, comprising the following steps of: repeatedly washing the polyamide textile in ultrasonic oscillation at the temperature of 60-90 DEG C by respectively using deionized water and absolute ethyl alcohol with mass concentration of 95%, and drying; then, processing the polyamide textile with the tetrabutyl titanate and the reactive dye; finally, washing the polyamide textile for 10-30 minutes with a cleaning solution at the temperature of 95 DEG C according to a bath ratio of 1:30-50, repeatedly washing the polyamide textile by respectively using hot water and cool water, and drying or naturally airing the polyamide textile to get the modified and dyed polyamide textile. With the method provided by the invention, production procedures are greatly simplified, material cost is saved, and additional value of products is improved. The modified and dyed polyamide textilehas excellent color fastness to dry and wet frictions, scrubbing and lighting; and polyamide textile has higher dye uptake and is dyed uniformly, after being washed for 30 times, the dyed polyamide textile still has better antibacterial property.

Description

technical field [0001] The invention belongs to the technical field of functional textile materials, and relates to a method for modifying and dyeing nylon fabric, in particular to a method for modifying and dyeing nylon fabric by using tetrabutyl titanate and reactive dyes. Background technique [0002] Nano-titanium dioxide is a very important inorganic semiconductor material. Its unique ultraviolet shielding ability, photocatalytic activity and color effect make it popular as soon as it comes out. It has broad applications in sun protection, sterilization, wastewater treatment, environmental protection and automobile industry application prospects. Fabrics with multiple functions can be prepared by utilizing the characteristics of nano-titanium dioxide such as high temperature resistance, refractory decomposition, non-toxicity, long-lasting function, and good compatibility with polymers. The preparation methods of nano titanium dioxide mainly include gas phase method, l...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06P1/38D06P3/24D06M11/46D06M101/34
Inventor 张辉朱红
Owner 福建金苑服饰有限公司
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