Modifying and dyeing method for polyamide textile by using tetrabutyl titanate and reactive dye
A technology of tetrabutyl titanate and reactive dyes, which is applied in dyeing methods, textiles and papermaking, fiber types, etc., can solve the problem that nano-titanium dioxide loading and dyeing cannot be realized simultaneously, nylon fabrics have low anti-ultraviolet and antibacterial properties, and fabric handles and poor air permeability, to achieve the effects of excellent color fastness to sunlight, saving raw materials, and high dyeing percentage
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Embodiment 1
[0028] Weigh 5g of nylon fabric and tetrabutyl titanate respectively, and weigh reactive brilliant blue X-BR dye according to 0.3% of the mass of nylon fabric, wherein the volume ratio of nylon fabric is 1:1 with deionized water and 95% anhydrous Ethanol solution, under the conditions of temperature 80°C, frequency 50KHz, power 100W, ultrasonic vibration washing for 30min, and drying at 60°C. Tetrabutyl titanate was dissolved in deionized water at a ratio of 1:80, reactive brilliant blue X-BR dye was added, and the nylon fabric was immersed in the mixed solution of tetrabutyl titanate dye for 10 minutes, and then the nylon fabric was mixed with titanium Add the aqueous solution of tetrabutyl acid dye to a 200ml high-temperature and high-pressure reactor, fill it with deionized water to 60% of the volume of the reactor, adjust the pH value to 6 with acetic acid, and keep the sealed reactor at 110°C for 6 hours. . After the reaction is over, wash with 2g / L soap flakes and 2g / L ...
Embodiment 2
[0031] Weigh 15g of nylon fabric and 5g of tetrabutyl titanate respectively, and weigh reactive brilliant blue X-BR dye according to 2% of the quality of nylon fabric, wherein the volume ratio of nylon fabric is 1:1 with deionized water and 95% Absolute ethanol solution, under the conditions of temperature 80°C, frequency 50KHz, power 100W, ultrasonic vibration washing for 30min, and drying at 60°C. Tetrabutyl titanate was dissolved in deionized water at a ratio of 1:120, reactive brilliant blue X-BR dye was added, and the nylon fabric was immersed in the mixed solution of tetrabutyl titanate dye for 5 minutes, and then the nylon fabric was mixed with titanium Add the aqueous solution of tetrabutyl ester dye to a 200ml high-temperature and high-pressure reactor, fill it with deionized water to 80% of the volume of the reactor, adjust the pH value to 4 with acetic acid, and keep the sealed reactor at 140°C for 3 hours. . After the reaction is over, wash with 2g / L soap flakes a...
Embodiment 3
[0034] Weigh 10g of nylon fabric and 5g of tetrabutyl titanate respectively, and weigh reactive brilliant blue X-BR dye according to 1% of the mass of nylon fabric, wherein the volume ratio of nylon fabric is 1:1 with deionized water and 95% Absolute ethanol solution, under the conditions of temperature 80°C, frequency 50KHz, power 100W, ultrasonic vibration washing for 30min, and drying at 60°C. Tetrabutyl titanate was dissolved in deionized water at a ratio of 1:100, reactive brilliant blue X-BR dye was added, and the nylon fabric was immersed in the mixed solution of tetrabutyl titanate dye for 8 minutes, and then the nylon fabric was mixed with titanium Add the aqueous solution of tetrabutyl ester dye to a 200ml high-temperature and high-pressure reactor, fill it with deionized water to 70% of the volume of the reactor, adjust the pH value to 5 with acetic acid, and keep the sealed reactor at 120°C for 5 hours. . After the reaction is over, wash with 2g / L soap flakes and ...
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