Method for preparing one-dimensional self-assembly material with ZnO nanorod array as template
A nanorod array and self-assembly technology, applied in nanotechnology, chemical instruments and methods, inorganic chemistry, etc., can solve problems such as film orientation and structural damage
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Embodiment 1
[0035] Embodiment 1: Preparation of zinc oxide nanorod array
[0036] The ZnO nanorod array with consistent orientation was prepared by traditional hydrothermal method. The specific method is as follows:
[0037] 1. Prepare 15ml each of 0.1M zinc nitrate and 0.1M hexamethylenetetramine solutions, and set aside;
[0038] 2. Add zinc nitrate and hexamethylenetetramine into a 50ml polytetrafluoroethylene hydrothermal kettle, and insert a cleaned substrate such as ITO glass or cordierite into the reaction solution at an angle of 45 degrees, and 95°C water Thermal reaction 4h.
[0039] 3. The scanning electron microscope photos of the prepared ZnO nanorod arrays are shown in figure 1 , as shown in the figure, the ZnO nanorods have a hexagonal columnar structure with a uniform growth orientation and an average diameter of 200 nm.
Embodiment 2
[0040] Example 2: Cerium Oxide Nanotube Arrays
[0041] 1. Preparation method: Immerse the zinc oxide nanorod array prepared in Example 1 into a 0.1M cerium nitrate solution, and conduct a hydrothermal reaction at a constant temperature of 95°C for 2 hours to obtain a cerium oxide nanorod with similar size and density as the zinc oxide nanorod array. tube array.
[0042] 2. The obtained cerium oxide: the scanning electron microscope photo of the prepared cerium oxide nanotube array is shown in figure 2 , as shown, the cerium oxide tubular structures have similar orientation and density to the ZnO nanorod arrays.
Embodiment 3
[0043] Embodiment 3: cobalt oxide nanotube array
[0044]1. Preparation method: immerse the zinc oxide nanorod array synthesized in Example 1 into a 0.16M cobalt nitrate solution, and conduct a hydrothermal reaction at 95° C. for 3 hours to obtain the cobalt oxide nanotube array.
[0045] 2. Obtained cobalt oxide: the scanning electron microscope photo of the prepared cobalt oxide nanotube array is shown in image 3 , image 3 As shown, the substrate is evenly distributed with a tubular array structure of cobalt oxide with uniform orientation.
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