Templet assembling technique of carbon-base nanotube coaxial heterojunction
A coaxial heterojunction, carbon-based nanotechnology, applied in the fields of carbon nanotubes, nanocarbons, nanotechnology, etc., can solve the problems of semiconductor characteristics characterization transistor assembly difficulties and other issues
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Embodiment 1
[0039] The technical route of the preparation process is as follows: figure 1 .
[0040] The product is a coaxial heterojunction of carbon-based nanotubes, which is formed by coaxial and seamless jointing of N-doped carbon-based nanotube segments and pure carbon nanotubes.
[0041] The controlled synthesis of the above carbon-based nanotube coaxial heterojunction uses anodized aluminum as a template, combined with chemical vapor deposition and plasma treatment. The main process steps are summarized as follows:
[0042] ①AAO template preparation: the channels are U-shaped, parallel to each other, and arranged in a directional manner. The openings are roughly located on the same plane, with an average diameter of 25nm and a depth of 5μm;
[0043] ② Preparation of N-doped carbon-based nanotubes: AAO templates were placed in an atmosphere protection furnace, and methyl nitrile (CH 3 CN) is the carbon source, high-purity nitrogen (volume purity ≥ 99.9996%, flow rate 500cm 3 / min...
Embodiment 2
[0049] The technical route of the preparation process is as follows: figure 1 .
[0050] The product is a coaxial heterojunction of carbon-based nanotubes, which is formed by coaxial and seamless jointing of pure carbon nanotube segments and N-doped carbon-based nanotube segments.
[0051] The controlled synthesis of the above carbon-based nanotube coaxial heterojunction uses anodized aluminum as a template, combined with chemical vapor deposition and plasma treatment. The main process steps are summarized as follows:
[0052] ① AAO template preparation: the channels are U-shaped, parallel to each other, arranged in a direction, and the openings are roughly located on the same plane, with an average diameter of 35nm and a depth of 1mm;
[0053] ②Preparation of pure carbon nanotubes: the AAO template is placed in an atmosphere protection furnace, and the reaction gas is acetylene (C 2 h 2 ) and high-purity nitrogen (N 2 ), a mixture of acetylene (C 2 h 2 ) and nitrogen (N...
Embodiment 3
[0060] The technical route of the preparation process is as follows: figure 2 .
[0061] The product is a coaxial heterojunction of carbon-based nanotubes, which is formed by coaxial and seamless jointing of pure carbon nanotube segments, N-doped carbon-based nanotubes and B-doped carbon-based nanotube segments.
[0062] The controlled synthesis of the above carbon-based nanotube coaxial heterojunction uses anodized aluminum as a template, combined with chemical vapor deposition and plasma treatment. The main process steps are summarized as follows:
[0063] ① AAO template preparation: the channels are hollow cylindrical, with openings at both ends, parallel to each other, and directional arrangement, the openings are roughly located on the same plane, with an average pore diameter of 20nm and a depth of 200nm;
[0064] ②Preparation of pure carbon nanotubes: the AAO template is placed in an atmosphere protection furnace, and the reaction gas is propylene (C 3 h 6 ) and hig...
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