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Method for preparing silicon carbide honeycomb ceramics

A technology of silicon carbide honeycomb and honeycomb ceramics, applied in ceramic products, applications, household appliances, etc., can solve the problems of insufficient strength, high reaction temperature, high specific surface area, etc., meet the requirements of guaranteed strength, reduce sintering temperature, and increase specific surface area. Effect

Active Publication Date: 2012-06-20
ZHEJIANG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Conventional silicon carbide honeycomb ceramics are prepared by making pores. The high reaction temperature leads to an increase in cost, which is not conducive to the realization of production. As a result, the purification of automobile exhaust is not enough, the air pollution cannot be effectively controlled, and there are still sintering performance and porous structure. The contradiction between the materials, such as the material has many holes but the strength is not enough, and the high specific surface area cannot be provided under the premise of ensuring the strength, so choosing new raw materials and processes to prepare silicon carbide honeycomb ceramics has become a new research direction

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] Embodiment 1, a kind of preparation method of silicon carbide honeycomb ceramics, carries out following steps successively:

[0039] 1), preparation of honeycomb ceramic powder:

[0040] Bamboo charcoal powder and industrial silica sol are used as aggregates, alumina and yttrium oxide are used as sintering aids, and potato starch is used as pore-forming agent;

[0041] Mix bamboo charcoal micropowder, industrial silica sol, aluminum oxide, yttrium oxide and potato starch in a weight ratio of 70:20:3:3:4; obtain honeycomb ceramic powder;

[0042] 2) Mixing mud:

[0043] Mix water, polyvinyl alcohol and polyhydroxyethanol in a weight ratio of 70:15:15, and stir evenly to obtain a solution;

[0044] Mix the solution with the honeycomb ceramic powder according to the weight ratio of 100:75, then fully knead in a mixer for 40 minutes under normal temperature and pressure, and stale for 2.5 hours under the same conditions (i.e. under normal temperature and pressure); get mu...

Embodiment 2

[0055] Embodiment 2, a kind of preparation method of silicon carbide honeycomb ceramics, carries out following steps successively:

[0056] 1), preparation of honeycomb ceramic powder:

[0057] Bamboo charcoal powder and industrial silica sol are used as aggregates, alumina and yttrium oxide are used as sintering aids, and potato starch is used as pore-forming agent;

[0058] Mix bamboo charcoal micropowder, industrial silica sol, aluminum oxide, yttrium oxide and potato starch in a weight ratio of 70:20:2:2:6; obtain honeycomb ceramic powder;

[0059] 2) Mixing mud:

[0060] Mix water, polyvinyl alcohol and polyhydroxyethanol in a weight ratio of 70:10:20, and stir evenly to obtain a solution;

[0061] Mix the solution with the honeycomb ceramic powder according to the weight ratio of 100:70, then fully knead in a mixer at normal temperature and pressure for 0.5 hours, and stale for 2 hours under the same conditions (i.e. under normal temperature and pressure); get mud ; ...

Embodiment 3

[0072] Embodiment 3, a kind of preparation method of silicon carbide honeycomb ceramics, carries out following steps successively:

[0073] 1), preparation of honeycomb ceramic powder:

[0074] Bamboo charcoal powder and industrial silica sol are used as aggregates, alumina and yttrium oxide are used as sintering aids, and potato starch is used as pore-forming agent;

[0075] Mix bamboo charcoal micropowder, industrial silica sol, aluminum oxide, yttrium oxide and potato starch in a weight ratio of 70:20:4:4:2; obtain honeycomb ceramic powder;

[0076] 2) Mixing mud:

[0077] Mix water, polyvinyl alcohol and polyhydroxyethanol according to the weight ratio of 70:14:16, and stir evenly to obtain a solution;

[0078] Mix the solution with the honeycomb ceramic powder according to the weight ratio of 100:78, then fully knead in a mixer for 45 minutes under normal temperature and pressure, and stale for 3 hours under the same conditions (i.e. under normal temperature and pressur...

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Abstract

The invention discloses a method for preparing silicon carbide honeycomb ceramics. The method comprises the following steps of: 1) mixing bamboo charcoal micro-powder, silica sol, aluminum oxide, yttrium oxide and organic matter starch at a weight ratio of 70: 20: (1-5): (1-5): (1-8), so as to obtain honeycomb ceramics powder; 2) mixing and pugging: mixing water, polyvinyl alcohol and polyhydroxyethanol according to a weight ratio of 70: (10-20): (10-20), and uniformly stirring the components to obtain a solution; and mixing the solution with the honeycomb ceramics powder according to a weight ratio of 100: (65-80), fully mixing the mixture in a mixing machine at a normal pressure and temperature for 0.5-1 hour, and then aging the mixture at the normal pressure and temperature for 2-3 hours, so as to obtain slurry material; 3) carrying out extrusion molding; 4) drying; and 5) sintering. The silicon carbide honeycomb ceramics produced by the preparation method disclosed by the invention has the characteristics of controllable holes, high specific surface area, intensity meeting requirements, and the like.

Description

technical field [0001] The invention relates to a method for preparing silicon carbide honeycomb ceramics, in particular to a method for preparing silicon carbide honeycomb ceramics with bamboo charcoal micropowder and industrial silica sol as aggregates. Background technique [0002] Honeycomb ceramics is a kind of porous functional material. As early as the 1970s, Corning Corporation of the United States began trial production. In 1975, the company had already used honeycomb ceramics to carry out small car exhaust purification tests, and obtained good effect. Honeycomb ceramics have high specific surface area and good physical and chemical stability. In addition, they also have low density, high permeability, good energy absorption performance, high temperature resistance, corrosion resistance, high chemical stability and dimensional stability, and easy regeneration. features. [0003] In recent years, with the continuous development of honeycomb ceramic preparation tech...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B38/06C04B35/565C04B35/622
Inventor 郭兴忠朱林杨辉
Owner ZHEJIANG UNIV
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