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Decomposition and filtration method during alumina production process

A filtration method and production process technology, applied in the direction of alumina/hydroxide, etc., can solve problems such as increased operating costs, cumbersome process transfers, increased investment, etc., to reduce investment costs and personnel operations, save intermediate links, The effect of saving land

Active Publication Date: 2012-06-27
NORTHEASTERN UNIV ENG & RES INST CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The decomposition area configuration of a traditional alumina plant is usually a decomposition tank system plus a seed filter plant. The output of the decomposition tank flows to the seed filter plant through the overflow pipe in the middle and upper part of the final decomposition tank to separate the mother liquor and seeds. The filtered seeds After the semen is diluted, it falls into the seed crystal tank under the seed filtration plant, and after stirring and mixing, the seed crystal pump is sent to the first decomposition tank; the overflow of the filter enters the overflow tank in the plant, and is sent to the first tank by the overflow pump. Decompose the end tank of the workshop; although this layout method is adopted by most domestic alumina plants, it also has the following disadvantages: (1) It occupies a large area and needs to build a separate seed filtration plant, and the general plan requires a special location for configuration; (2) The increase in cost investment requires not only the production of a larger plant frame, but also the configuration of corresponding auxiliary equipment such as: seed tanks, seed pumps, overflow tanks, overflow pumps, etc., and the cost of civil engineering and equipment increases; (3 ) The operating cost increases, and the seed tank, seed pump, overflow tank, and overflow pump increase the power load consumption and equipment maintenance work; The conversion from the pump to the first decomposition tank, and from the overflow tank to the overflow pump, and from the overflow pump to the final decomposition tank increases the workload of the on-site operators and reduces the work efficiency; (5) It is not good for the process itself, because from the general layout In general, there is a certain distance between the decomposition and seed filtration workshops. Therefore, most of the takeover of the decomposition and seed filtration workshops needs to be connected with the outdoor pipe network, and the investment of the outdoor pipe network in pipes and pipe racks will increase accordingly.
Sometimes due to configuration problems, the pipeline runs far away, and the slurry pipeline will be blocked in the middle

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] The structure of the decomposition and filtration system in the alumina production process is as follows: figure 1 As shown, the decomposition tank system is composed of 12 decomposition tanks connected in series including the first decomposition tank 1, the second decomposition tank 2, the penultimate decomposition tank 3 and the final decomposition tank 4; the vertical disc filter 5, the vacuum liquid receiving tank 6 And the gas-liquid separator 7 is arranged above the first decomposition tank 1;

[0025] The two distribution heads of the vertical disc filter 5 communicate with the vacuum liquid receiving tank 6, the air outlet at the top of the vacuum liquid receiving tank 6 communicates with the gas-liquid separator 7, and the air suction port above the gas-liquid separator 7 communicates with the vacuum pump 12;

[0026] A liquid outlet is provided below the vacuum liquid receiving tank 6 and the gas-liquid separator 7, and a mother liquor buffer tank 8 is provide...

Embodiment 2

[0041] The structure of the decomposition and filtration system in the alumina production process is different from that of Embodiment 1 in that the decomposition tank system is composed of 14 decomposition tanks connected in series;

[0042] The working method differs from Example 1 in that: the temperature of the slurry decomposed in the penultimate decomposition tank is 48-50°C, its solid content is 780g / L, the content of alumina is 105g / L, and the content of sodium hydroxide is 182g / L;

[0043] The content of aluminum oxide in cold semen is 190g / L, and the content of sodium hydroxide is 165g / L;

[0044] The water content of the filter cake filtered by the vertical disc filter is 25%, and the solid content after mixing with cold semen is about 780g / L;

[0045] The decomposition time of the filter cake diluted with cold semen in the decomposition tank system is 50h;

[0046] The solids content of the underflow of the classifying cyclone was 800 g / L.

Embodiment 3

[0048] The structure of the decomposition and filtration system in the alumina production process is the same as in Embodiment 1, the difference being that the decomposition tank system is composed of 16 decomposition tanks connected in series;

[0049] The working method is the same as in Example 1, the temperature of the slurry decomposed in the penultimate decomposition tank is 48~50°C, its solid content is 820g / L, the content of alumina is 100g / L, and the content of sodium hydroxide is 178g / L ;

[0050] The content of aluminum oxide in cold semen is 195g / L, and the content of sodium hydroxide is 170g / L;

[0051] The water content of the filter cake filtered by the vertical disc filter is 30%, and the solid content after mixing with cold semen is about 820g / L;

[0052]The decomposition time of the filter cake diluted with cold semen in the decomposition tank system is 52 hours;

[0053] The solids content of the underflow of the classifying cyclone was 900 g / L.

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Abstract

A decomposition and filtration method during the alumina production process belongs to the technical field of alumina production. A vertical disc filter, a vacuum liquid receiving tank and a gas-liquid separation device are arranged over a first decomposer of a decomposer system. The method provided by the invention comprises the following steps of: allowing aluminium hydroxide slurry in a last decomposer of the decomposer system to enter into the vertical disc filter, pumping and back-flushing the vertical disc filter, separating a filter cake and decomposing a mother liquor, allowing a cold seminal fluid to enter into the vertical disc filter to dilute the unloaded filter cake, discharging the diluted filter cake into the first decomposer of the decomposer system by the utilization of potential difference, and allowing an overflow of the vertical disc filter to enter into the last decomposer. By the utilization of potential difference, the diluted filter cake is directly conveyed into the first decomposer from the vertical disc filter, thus simplifying the flow and saving land occupation, equipment investment and power consumption.

Description

technical field [0001] The invention belongs to the technical field of alumina production, in particular to a decomposition and filtration method in the alumina production process. Background technique [0002] The decomposition area configuration of a traditional alumina plant is usually a decomposition tank system plus a seed filter plant. The output of the decomposition tank flows to the seed filter plant through the overflow pipe in the middle and upper part of the final decomposition tank to separate the mother liquor and seeds. The filtered seeds After the semen is diluted, it falls into the seed crystal tank under the seed filtration plant, and after stirring and mixing, the seed crystal pump is sent to the first decomposition tank; the overflow of the filter enters the overflow tank in the plant, and is sent to the first tank by the overflow pump. Decompose the end tank of the workshop; although this layout method is adopted by most domestic alumina plants, it also h...

Claims

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Application Information

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IPC IPC(8): C01F7/02
Inventor 鄢艳郭建强
Owner NORTHEASTERN UNIV ENG & RES INST CO LTD