Active packaging film for chilled meat and preparation method of the active packaging film
A technology for packaging film and chilled meat, applied in the field of active packaging film and its preparation, can solve the problems that the growth of chilled meat cannot be inhibited, cannot be naturally degraded, has no biological activity, etc. Delicate and fresh-keeping effect
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Embodiment 1
[0040] Preparation of sustained-release microcapsules:
[0041] Weigh a certain amount of 8g β-cyclodextrin, add 64ml of deionized water in a weight ratio of 1:8, heat, and after the β-cyclodextrin dissolves, add clove essential oil, the amount of which is the weight of β-cyclodextrin 1 / 6 of that, wherein the essential oil is dissolved in ethanol with a mass concentration of 70% in advance, and the ratio of essential oil to ethanol is 1:10. Take out the β-cyclodextrin solution added with essential oil at 70°C and 700r / min for 1-1.5h, then take it out, cool it to room temperature, put it in a refrigerator at 5°C for 24h, vacuum filter, and remove the filter residue Rinse with 20ml each of deionized water and ethanol. The filter residue was collected and dried in a blast drying oven at 50°C to constant weight to obtain sustained-release microcapsules.
[0042] Preparation of active antibacterial film for chilled meat:
[0043] Take 40g of PVA, 1g of SDS and 8ml of ethylene gl...
Embodiment 2
[0052] The preparation of slow-release microcapsules: with embodiment 1.
[0053] Preparation of active antibacterial film for chilled meat:
[0054] Take 40g of PVA, 1g of SDS and 8ml of ethylene glycol in a 500ml beaker, add 250ml of water. The beaker was placed in a constant temperature water bath and heated to 60°C under low-speed stirring to obtain dispersion A. Weigh 4g of microcapsules into a 250ml beaker, add 50ml of water, and place the beaker in an ultrasonic oscillator for 15 minutes until the microcapsules are more evenly dispersed in water to obtain dispersion B. Slowly add dispersion B to dispersion A to obtain dispersion C. Continue to heat the dispersion C to 95°C-100°C under low-speed stirring until the PVA is completely melted, take it out and cool it to about 60°C. Weigh 10g PLA and dissolve it in 200ml DMSO to obtain solution D, add solution D to solution C, mix well and defoam in vacuum to obtain solution E. Pour liquid E into the hopper of the cast fi...
Embodiment 3
[0060] The preparation of slow-release microcapsules: with embodiment 1.
[0061] Preparation of active antibacterial film for chilled fresh meat:
[0062] Take 40g of PVA, 1g of SDS and 8ml of ethylene glycol in a 500ml beaker, add 250ml of water. The beaker was placed in a constant temperature water bath and heated to 60°C under low-speed stirring to obtain dispersion A. Weigh 4g of microcapsules into a 250ml beaker, add 50ml of water, and place the beaker in an ultrasonic oscillator for 15 minutes until the microcapsules are more evenly dispersed in water to obtain dispersion B. Slowly add dispersion B to dispersion A to obtain dispersion C. Continue to heat the dispersion C to 95°C-100°C under low-speed stirring until the PVA is completely melted, take it out and cool it to about 60°C. Weigh 8g PLA and dissolve it in 200ml DMSO to obtain solution D, add solution D to solution C, mix well and defoam in vacuum to obtain solution E. Pour liquid E into the hopper of the ca...
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