Production method for corona resistant enamel wire
An enameled wire varnish and production method technology, which is applied in the chemical industry, coating, climate sustainability, etc., can solve the problems of precipitation layering and large dispersion of product performance, and achieve low production cost, good corona resistance, Simple process and reliable results
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Embodiment 1
[0017] Take 19.92kg of isophthalic acid, 7.1kg of ethylene glycol, and 1.1kg of glycerol, put them into a 50-liter reactor with a fractionation dehydration column, fill with carbon dioxide gas, and start stirring under the condition of a pressure of 0.2MPa (gauge pressure) Heat up the temperature to 180°C, then rise to 220°C at a constant speed for about four hours, remove the pressure, make the system under normal pressure, raise the temperature at a rate of 8-12°C per hour, raise the temperature to 240°C, keep warm and take samples to measure the acid value , when the acid value drops to 120mg / g, start to drop the temperature, the temperature drops to 100°C, open the bottom valve of the reactor to obtain polyester with a low degree of polymerization. The appearance of the product is a colorless or yellowish viscous fluid. Its viscosity is about 10 Pas.
[0018] Put the material in the previous step into a high-speed mixer, add 5 kg of nano-silica powder particles treated wi...
Embodiment 2
[0024] Adopt nano-titanium dioxide powder particles, mix with 1wt% titanate coupling agent in a high-speed mixer, after activation treatment, replace the nano-silica powder particles treated with silane in Example 1, other process conditions and implementation Example 1 is the same. The appearance of the prepared product is an opaque white viscous slurry. After standing for half a year, no signs of powder particle aggregation, agglomeration or sedimentation and stratification were found. Samples were taken from various containers storing the product to measure the density. The degree of uneven density of the samples If it is less than 2%, it means that the dispersion state of the powder material is stable; the enameled wire is made by coating copper wire with a general-purpose enameled wire coating machine. Under the conditions of 100ns, 20kHz, 3kV, and 155°C, the frequency conversion resistance life exceeds 50 hours.
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