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Non-fluorescent anti-collapse fluid loss agent for drilling fluid and production process

A fluid loss reducing agent, non-fluorescence technology, applied in drilling compositions, chemical instruments and methods, etc., can solve the problems such as large influence on drilling fluid performance, low temperature resistance, environmental pollution, etc. No adverse effect on performance, reduced frictional resistance, good effect of plugging cracked layers

Active Publication Date: 2014-08-20
河北华运鸿业化工有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the commonly used anti-slumping agents include polyols, natural asphalt and inorganic salts. Among them, the cost of anti-slumping agents of polyols is relatively high, and some products have a great impact on the performance of drilling fluids, causing foaming; inorganic salts The cost of anti-slumping agent is low, but it increases the annual and filtration loss of drilling fluid, which seriously affects the performance of drilling fluid; natural asphalt anti-slumping agent has better plugging performance, but it has fluorescence, so it is not suitable for exploration wells and pre-exploration wells used in
FT-342, a representative of natural asphalt anti-slump agent, consists of vegetable oil, mineral oil, natural asphalt sulfonate, coating inhibitor and surfactant; this anti-slump agent not only has fluorescence, but also has relatively high temperature resistance. Low, usually only 150°C~180°C, and the anti-slump performance and filter reduction effect are not outstanding, and the compatibility with other drilling fluids is poor, which is easy to cause pollution to the environment

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] A non-fluorescent anti-slump fluid loss additive for drilling fluids, comprising the following components in parts by weight:

[0018] 100 parts of natural asphalt; 50 parts of white oil; 50 parts of diesel oil; 2 parts of NP-9 alkylphenol polyoxyethylene (9) ether; 2 parts of dodecylbenzenesulfonic acid; 60 parts of sulfonated phenolic resin; polyacrylamide 20 parts, UV absorber (UV-9) 1 part.

[0019] The production process of the above-mentioned non-fluorescent anti-slump fluid loss reducing agent for drilling fluid comprises the following steps:

[0020] a. put the natural asphalt in the reaction kettle, add white oil, diesel oil, NP-9 alkylphenol polyoxyethylene (9) ether, dodecylbenzenesulfonic acid and ultraviolet absorber successively in the natural asphalt, heat up to Keep at 60°C, stir at constant temperature for 1h;

[0021] b. Add polyacrylamide to the solution in step a, and stir at constant temperature for 30 minutes;

[0022] c. Add sulfonated phenolic...

Embodiment 2 to Embodiment 9

[0026] The components of the non-fluorescent anti-slump fluid loss agent in Examples 2 to 9 are the same as in Example 1, and the weight percentages of each component are shown in Table 1.

[0027] Table 1

[0028] components Example 2 Example 3 Example 4 Example 5 Example 6 Example 7 Example 8 Example 9 natural asphalt 100 100 100 100 100 100 100 100 white oil 40 42 46 48 53 55 58 60 diesel fuel 47 55 42 60 56 51 49 40 NP-9 1.2 2.0 2.5 3.0 2.6 1.8 1.5 1.0 dodecylbenzenesulfonic acid 2.5 2.6 2.2 2.0 1.8 1.6 1.4 1.0 Sulfonated phenolic resin 52 65 50 60 70 68 62 55 polyacrylamide 15 30 16 12 18 10 29 24 UV absorber 1 1 1 1 1 1 1 1

[0029] The production process steps of Embodiment 2 to Embodiment 9 are also the same as Embodiment 1, and the specific parameter settings in the process are shown in Table 2.

[0030] Table 2

[0031] step ...

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PUM

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Abstract

The invention discloses a non-fluorescent anti-slump fluid loss agent for drilling fluid, which comprises the following components in parts by weight: 100 parts of natural asphalt; 40-60 parts of white oil; 40-60 parts of diesel oil; NP-9 alkyl 1~3 parts of phenol polyoxyethylene (9) ether; 1~3 parts of dodecylbenzenesulfonic acid; 50~70 parts of sulfonated phenolic resin; 10~30 parts of polyacrylamide, 1 part of ultraviolet absorber. The anti-slump and fluid loss reducing agent prepared by the invention is applied in drilling fluid, and has the characteristics of high temperature resistance, high oil solubility, and good plugging and fluid loss reducing effects.

Description

technical field [0001] The invention relates to an anti-slump agent for drilling fluid and a production process of the anti-slump agent. Background technique [0002] Wellbore instability during drilling has always been the main factor affecting the smooth progress of drilling, especially in the case of increasing number of deep wells, ultra-deep wells, directional wells and highly deviated wells, the above problems are more prominent. During the drilling construction process, People often add anti-slump agent and fluid loss reducer to solve the above problems. At present, the commonly used anti-slumping agents include polyols, natural asphalt and inorganic salts. Among them, the cost of anti-slumping agents of polyols is relatively high, and some products have a great impact on the performance of drilling fluids, causing foaming; inorganic salts The cost of anti-slumping agent is low, but it increases the annual and filtration loss of drilling fluid, which seriously affect...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K8/035
Inventor 张占山张学良张学军
Owner 河北华运鸿业化工有限公司
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