Environment-friendly wall material for interior wall decoration and preparation method of wall material
An environmentally friendly wall material and interior wall technology, applied in the field of interior wall decoration wall material and its preparation, can solve the problems of difficult to reuse, uneven distribution, low decomposition efficiency, etc., to prevent the generation of mold, prevent excessive dryness or humidity , The effect of purifying indoor air
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[0039] Example 1:
[0040] 1. Preparation of diatomaceous earth
[0041] Take 100 g of diatomaceous earth and grind it with a ball mill at 200 rpm for 1 hour. After separating and removing larger impurity particles with a 200 mesh screen, add 400 g of water, stir for 30 min, and let stand for 10 min. The upper turbid liquid is sucked out, and then the turbid liquid is filtered. Put the filter cake into a beaker, add a 35% concentration of hydrochloric acid solution, stir at 70°C at 200 rpm for 1 hour, and put it into a 150W ultrasonic cleaner. After 2h, adjust the pH value of the diatomaceous earth suspension to 3, take it out, filter, wash, and dry the filter cake in vacuum at 120℃ for 2h, then put it in a muffle furnace and calcinate at 600℃ for 2h, that is, it has a high specific surface area after expansion. For the scanning electron microscope (SEM) image and energy spectrum analysis (EDAX) image of diatomite with high porosity, please refer to the attached figure 1 (a) and a...
Example Embodiment
[0056] Example 2:
[0057] According to the method in Example 1, the original diatomaceous earth was expanded to obtain a diatomaceous earth with a high specific surface area.
[0058] Mix 25 ml of absolute ethanol with 10 ml of butyl titanate, stir at 200 rpm for 10 min, add 20 g of diatomaceous earth, and stir vigorously for 10 min to form a slurry. Add 4ml of glacial acetic acid and 10ml of distilled water to 35ml of absolute ethanol, stir at 400rpm for 10min and add hydrochloric acid to adjust the pH of the solution to 2. Under stirring, the above solution was slowly dropped into the diatomaceous earth slurry, and the addition was completed for 10 minutes, and stirred at 400 rpm for 30 minutes and ultrasonically vibrated for 1 hour. Let it stand in a water bath at 50°C for 24h. After the material forms a gel and cannot flow, it is vacuum dried at 60°C for 3h, and calcined in a muffle furnace at 450°C for 2h to obtain titanium-loaded diatomaceous earth.
[0059] Dip 20g diatomac...
Example Embodiment
[0062] Example 3:
[0063] According to the method in Example 1, the original diatomaceous earth was subjected to capacity expansion treatment to obtain diatomaceous earth with high specific surface area.
[0064] Mix 35 ml of absolute ethanol with 10 ml of butyl titanate, stir at 200 rpm for 10 min, add 20 g of diatomaceous earth, and stir vigorously for 10 min to form a slurry. Add 4ml of glacial acetic acid and 10ml of distilled water to 25ml of absolute ethanol, stir at 400rpm for 10min, add hydrochloric acid to adjust the pH of the solution to 2. Under stirring, the above solution was slowly dropped into the diatomaceous earth slurry, and the addition was completed in 10 minutes, and stirred at 400 rpm for 30 minutes and ultrasonically vibrated for 30 minutes. Let it stand in a water bath at 50°C for 24h. After the material forms a gel and cannot flow, it is vacuum dried at 60°C for 2h, and calcined in a muffle furnace at 480°C for 2h to obtain titanium-loaded diatomite.
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