Method for preparing hydrogen in process of producing manganous-manganic oxide through electrolytic manganese metal
A technology for electrolysis of manganese metal and manganese tetroxide, applied in the production of manganese oxide/hydroxide, hydrogen, etc., can solve the problems of direct hydrogen emission and high hydrogen concentration, and achieve energy saving, low economic cost and good economic benefits Effect
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[0018] Example 1
[0019] (1) Weigh 1000g of electrolytic metal manganese, crush it in a ball mill for 1 hour to produce electrolytic metal manganese powder 1, and use an analytical sieve to detect that its particle size is 100% less than 100μm;
[0020] (2) Add 3L of distilled water to electrolytic manganese metal powder 1 to prepare slurry 2, and put slurry 2 into the hydrogen generator;
[0021] (3) Weigh 10g of ammonium chloride, add it to slurry 2, control the system temperature at 65°C, stir the reaction for 1h, discharge the gas released by the reaction in the first 3 minutes, use a collection bag to collect the gas released by the subsequent reaction 3, Slurry 2 generates manganese hydroxide after hydrolysis;
[0022] (4) The manganese hydroxide is oxidized with compressed air at a temperature of 60°C. After a reaction time of 6 hours, trimanganese tetraoxide 4 is prepared;
[0023] (5) The trimanganese tetraoxide 4 is washed and dried to obtain trimanganese tetraoxide product ...
Example Embodiment
[0025] Example 2
[0026] (1) Weigh 2000g of electrolytic metal manganese, crush it in a ball mill for 1.5 hours to produce electrolytic metal manganese powder 1, and use an analytical sieve to detect that its particle size is 100% less than 75μm;
[0027] (2) Add 5L of distilled water to the electrolytic manganese metal powder 1 to prepare slurry 2 and put the slurry 2 into the hydrogen generator;
[0028] (3) Weigh 25g of ammonium sulfate, add it to slurry 2, control the system temperature at 80℃, stir the reaction for 1 hour, discharge the gas released by the reaction in the first 3 minutes, use a collection bag to collect the gas released by the subsequent reaction 3, slurry Material 2 generates manganese hydroxide after hydrolysis;
[0029] (4) The manganese hydroxide is oxidized with compressed air at a temperature of 60°C. After a reaction time of 6 hours, trimanganese tetraoxide 4 is prepared;
[0030] (5) The trimanganese tetraoxide 4 is washed and dried to obtain trimanganese...
Example Embodiment
[0032] Example 3
[0033] (1) Weigh 1500g of electrolytic metal manganese, add 4L of distilled water to make slurry 1;
[0034] (2) Put slurry 1 in a ball mill for 1 hour to make slurry 2, and put slurry 2 in a hydrogen generator;
[0035] (3) Weigh 20g of manganese chloride, add slurry 2, control the system temperature at 85°C, stir for 1 hour, and discharge the gas released during the first 3 minutes of reaction. Use a collecting bag to collect the gas released by the subsequent reaction. Material 2 generates manganese hydroxide after hydrolysis;
[0036] (4) The manganese hydroxide is oxidized with compressed air at a temperature of 60°C. After a reaction time of 6 hours, trimanganese tetraoxide 4 is prepared;
[0037] (5) The trimanganese tetraoxide 4 is washed and dried to obtain trimanganese tetraoxide product 5.
[0038] Finally, the gas 3 is monitored with a portable hydrogen purity analyzer HCKDGPH2-M, where the hydrogen content is 81%. The manganese tetroxide product 5 can be...
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