Phenyl phosphonic acid rare-earth salt compounded system flame-retardant glass fiber enhanced PET material and preparation method thereof
A technology of polyethylene terephthalate and polyethylene terephthalate, which is applied to the flame-retardant glass fiber reinforced polyethylene terephthalate material of phenylphosphonic acid rare earth salt compound system and the same In the field of preparation, it can solve the problems of weakened dominant position and toxicity, and achieve the effect of obvious effect, simple and easy processing method, and wide application range.
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[0043] The formula of the example is as follows:
[0044] (2) In this example, the rare earth element lanthanum (La) was used as an example to synthesize lanthanum phenylphosphonate (LaPP) for experimentation. The method for synthesizing lanthanum phenylphosphonate is the preparation method of the rare earth phenylphosphonate salt, specifically : (1) Add 8mmol phenylphosphonic acid (H 2 O 3 PC 6 H 5 ,) Dissolve in 100mL ethanol / water mixed solvent (ethanol / water volume ratio 1:1) to obtain a phenylphosphonic acid solution, and then place the resulting solution in a 250mL three-necked flask;
[0045] (2) Take 8mmol ReCl 3 ·6H 2 O was dissolved in 75mL of deionized water and added to the phenylphosphonic acid solution of step (1), stirred, adjusted to pH 6 with 0.1mol / L NaOH solution, stirred and refluxed at 70~80℃ for 22 hours to obtain White suspension
[0046] (3) The white suspension obtained in step (2) is suction filtered, washed with deionized water, filtered, and dried at 80°C...
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